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AOAC Final Action Method 2016.02 (Biotin)
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Table 2016.02D: Biotin (µg/100g) Practice Samples
Lab #
PRACTICE Sample 1
PRACTICE Sample 2
A
B
A
B
1
39.28
39.28
15.50
15.50
2
37.76
38.74
14.69
15.68
3
40.21
40.21
15.11
15.11
4
39.40
39.40
15.17
15.17
5
42.90
37.30
13.20
15.90
6
39.33
39.92
14.73
15.79
7
31.73
32.26
12.38
11.50
8
40.49
40.38
15.98
16.48
9
40.83
40.61
14.41
15.53
10
38.58
38.58
14.73
14.73
11
39.80
39.10
15.10
15.30
12
34.29
35.89
16.00
14.87
Mean
38.72
38.47
14.75
15.13
%RSD
7.75
6.17
7.14
8.19
Table 2016.02E: Biotin (µg/100g) MLT samples (Day 1)
Lab #
MLT Sample 1
MLT Sample 2
MLT Sample 3
MLT Sample 4
MLT Sample 5
MLT Sample 6
A
B
A
B
A
B
A
B
A
B
A
B
1
32.96
31.42
68.94
72.48
3.45
3.88
70.84
73.68
24.42
24.78
46.79
43.44
2
39.47
38.48
81.71
83.53
4.33
4.49
78.33
68.43
27.42
28.91
51.02
48.20
3
33.38
33.21
80.37
81.62
4.03
4.22
69.58
72.92
26.25
27.38
46.18
45.42
4
35.41
34.62
81.88
80.43
3.79
3.74
71.65
70.80
28.39
24.24
44.15
44.03
5
37.49
34.70
84.88
79.87
3.84
4.37
77.67
74.07
26.12
25.93
47.15
43.55
6
29.09
35.06
77.44
81.29
4.43
4.05
74.44
74.98
29.29
32.95
41.88
47.62
7
33.45
32.33
76.96
75.88
4.29
3.96
57.51
59.17
24.82
24.66
39.25
41.15
8
27.85
30.34
75.70
79.96
3.66
4.00
72.86
70.76
25.36
30.22
39.91
45.41
9
34.96
37.95
81.26
81.41
4.33
4.43
74.23
74.41
27.94
26.37
42.89
47.41
Mean
33.78
34.23
78.79
79.61
4.02
4.13
71.90
71.02
26.67
27.27
44.36
45.14
%RSD
10.89
8.04
5.95
4.24
8.68
6.37
8.53
6.94
6.31
10.72
8.57
5.16
Table 2016.02F: Biotin (µg/100g) MLT Samples (Day 2)
Lab #
MLT Sample 7
MLT Sample 8
MLT Sample 9
MLT Sample 10 MLT Sample 11 MLT Sample 12
A
B
A
B
A
B
A
B
A
B
A
B
1
195.27 200.37 270.20 265.83 171.08 155.73 10.69
9.80
44.26
44.68
48.66
56.39
2
200.63 191.30 271.16 266.46 180.38 159.53 11.11
10.68
46.01
43.08
52.02
53.47
3
196.99 196.48 265.19 272.41 179.63 168.93 10.40
10.24
42.19
43.96
54.56
54.37
4
191.31 205.32
251.11
265.49 171.89 162.31 11.19
9.20
44.02
44.66
54.54
54.92
5
196.80 196.60 260.67 247.84 170.46 161.75
9.76
9.37
40.82
40.13
52.48
49.79
6
193.53 186.75 263.54 248.41 184.86 161.43
9.88
9.89
43.31
42.48
53.84
56.11
7
185.41 190.38 219.30 213.21 153.16 140.19 10.05
9.15
38.43
39.03
50.09
50.14
8
201.99 199.82 268.69 254.35 175.94 163.60
9.36
9.59
40.44
42.14
52.00
44.45
9
202.58 205.62 278.04 274.41 183.98 158.33 11.02
10.72
46.05
46.44
55.47
54.89
Mean
196.06 196.96 260.88 256.49 174.60 159.09 10.38
9.85
42.84
42.96
52.63
52.73
%RSD
2.81
3.33
6.64
7.37
5.55
5.02
6.35
6.02
6.05
5.42
4.24
7.39
2016.02 (BIOTIN) FINAL ACTION REVIEW
FOR ERP USE ONLY
DO NOT DISTRIBUTE
209