103 / 164
Precision
Accuracy
Table 3
Product
SPIFAN Code Analyte
Nr. replicates (n) Conc. Level
RSDr
RSD iR
Conc. Level
RSDr
RSD iR
SRM1849a
CLC10-B Tryptophan
12
20.1
0.4
1.5
X
≤Z % ≤W%
Infant Formula Powder Partially Hydrolyzed Milk Based 410057652Z Tryptophan
12
25.3
0.6
1.0 Analyte 1
0.4-5.0
4%
Infant Formula Powder Partially Hydrolyzed Soy Based
410457651Z Tryptophan
12
18.3
5.0
6.9 Analyte 2
Toddler Formula Powder Milk-Based
4052755861 Tryptophan
12
25.7
0.8
2.0 Analyte 3
Infant Formula Powder Milk-Based
4044755861 Tryptophan
12
24.1
0.2
1.8 Analyte 4
Adult Nutritional Powder Low Fat
00859RF00 Tryptophan
12
21.4
0.9
1.7 Analyte 5
Child Formula Powder
00866RF00 Tryptophan
12
23.7
0.9
1.3 Analyte 1
5.0-50
3%
Infant Elemental Powder
00795RF Tryptophan
12
32.2
0.2
1.6 Analyte 2
Infant Formula Powder FOS/GOS Based
50350017W1 Tryptophan
12
23.2
2.0
2.4 Analyte 3
Infant Formula Powder Milk Based
K16NTAV Tryptophan
12
19.5
0.3
1.7 Analyte 4
Infant Formula Powder Soy Based
E10NWZC Tryptophan
12
18.3
0.2
2.3 Analyte 5
Infant Formula RTF Milk Based
EV4H2R Tryptophan
12
22.4
0.5
1.8 Analyte 1
50-2500
2%
Adult Nutritional RTF High Prtotein
00730RF00 Tryptophan
12
70.6
1.9
3.7 Analyte 2
Adult Nutritional RTF High Fat
00729RF00 Tryptophan
12
91.3
0.3
1.9 Analyte 3
Analyte 4
Analyte 5
Analyte 1
Analyte 2
Analyte 3
Analyte 4
Analyte 5
Global Mean %
1.0
2.3
Precision - repeatability.
REQUIREMENTS SMPR
Table 1
Accuracy - Spike Recovery
Avg (%) RSD % Avg (%) RSD (%)
SRM1849a
CLC10-B
TRP
12
20.1
99.9
1.8
100.9
2.4
Infant Formula Powder Partially Hydrolyzed Milk Based
410057652Z
TRP
12
25.3
104.3
3.3
104.1
2.7
Infant Formula Powder Partially Hydrolyzed Soy Based
410457651Z
TRP
11
18.3
103.7
8.6
101.5
4.8
Adult Nutritional Powder Low Fat
00859RF00
TRP
12
21.4
96.2
5.2
99.5
3.9
Infant Elemental Powder
00795RF
TRP
10
32.2
100.7
2.5
102.4
2.7
Infant Formula Powder Milk Based
K16NTAV
TRP
12
19.5
100.5
3.0
101.7
2.0
Infant Formula Powder Soy Based
E10NWZC
TRP
12
18.3
93.8
5.1
99.5
3.5
Adult Nutritional RTF High Fat
00729RF00
TRP
12
91.3
104.8
1.6
104.9
1.3
Global Mean % 100.5
3.9 101.8
2.9
+ Spike Level 1
SPIFAN Code
+ Spike Level 2
Spike Recovery
Product
Nr. replicates (n)
Native level
Analyte
AMINO-02 (FEBRUARY 2017)
SLV - FINAL REPORT
FOR ERP USE ONLY
DO NOT DISTRIBUTE
9