AOAC SPIFAN Review Team (February 2017)

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Single Laboratory Validation Report for Total Amino Acids by UHPLC-UV in Infant Formulas and Adult Nutritionals - APPENDICES
Jaudzems, Lahrichi, and Fuerer – January 2017 page 21/22
SPIFAN II SLV kit product #17: Infant Formula RTF Milk Based
SPIFAN II SLV kit product #18: Adult Nutritional RTF High Protein
1.317 2.140
AMQ - 2.813
NH3 - 3.337
His - 3.745
Tau - 4.930 6.146
Ser - 6.276
Arg - 7.279
Gly - 7.700
7.8888.173
Asp - 9.461
10.835
Glu - 12.183
12.956
Thr - 13.624
14.355
Ala - 14.640
Pro - 15.765
15.941 16.02516.168 16.516 16.592 16.659 16.848
Deriv Peak - 16.976
17.114
Lys - 17.284
Tyr - 17.654
xCys - 17.938Met - 18.042
Val - 18.314NVa - 18.616
18.90819.10519.438 19.864
Ile - 20.096
Leu - 20.317
Phe - 20.607
20.946
21.75521.850
AU
0.000
0.005
0.010
0.015
0.020
0.025
0.030
0.035
0.040
0.045
0.050
0.055
0.060
0.065
0.070
0.075
0.080
Minutes
1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00
2.246
AMQ - 3.019
NH3 - 3.647
His - 4.229
mono-LYS - 5.267Tau - 5.590 6.4686.770
Ser - 7.100 Arg - 8.369
Gly - 8.644
9.155
Asp - 10.609
11.04511.307
Glu - 12.873
13.459
Thr - 14.009
Ala - 14.910
Pro - 15.945
16.59416.768
Deriv Peak - 17.078
Cys - 17.193
Lys - 17.385
17.532
Tyr - 17.795
xCys - 18.073 Met - 18.169
Val - 18.419
NVa - 18.719
18.986 19.504
Ile - 20.176
Leu - 20.391
Phe - 20.700
20.998
21.76421.876
AU
0.000
0.010
0.020
0.030
0.040
0.050
0.060
0.070
0.080
0.090
0.100
0.110
0.120
0.130
0.140
0.150
Minutes
1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00
AMINO-01 (FEBRUARY 2017) - APPENDICES
FOR ERP USE ONLY
DO NOT DISTRIBUTE