AOAC SPIFAN Review Team (February 2017)

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Single Laboratory Validation Report for Total Amino Acids by UHPLC-UV in Infant Formulas and Adult Nutritionals - APPENDICES
Jaudzems, Lahrichi, and Fuerer – January 2017 page 20/22
SPIFAN II SLV kit product #15: Infant Formula Powder Milk Based
SPIFAN II SLV kit product #16: Infant Formula Powder Soy Based
1.319 2.144
AMQ - 2.816
NH3 - 3.341
His - 3.751
Tau - 4.933 6.152
Ser - 6.279
Arg - 7.281Gly - 7.702
8.177
Asp - 9.460
10.837 11.318 11.668
Glu - 12.181
12.947
Thr - 13.623
Ala - 14.639
Pro - 15.764
15.944 16.515 16.591 16.847
Deriv Peak - 16.976
17.115
Lys - 17.284
Tyr - 17.654
xCys - 17.938Met - 18.042
Val - 18.314
NVa - 18.616
18.90919.10519.261
Ile - 20.097
Leu - 20.318
20.500
Phe - 20.608
20.945
21.75721.850
21.971
AU
0.000
0.005
0.010
0.015
0.020
0.025
0.030
0.035
0.040
0.045
0.050
0.055
0.060
0.065
0.070
0.075
0.080
Minutes
1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00
1.320 2.143
AMQ - 2.818
NH3 - 3.342
His - 3.753
Tau - 4.935 6.146
Ser - 6.283
Arg - 7.285
Gly - 7.705
8.182
Asp - 9.460
10.833
Glu - 12.177
12.944
Thr - 13.620
Ala - 14.638
Pro - 15.764
15.937 16.516 16.592 16.659
Deriv Peak - 16.976
17.115
Lys - 17.285
Tyr - 17.655
xCys - 17.938Met - 18.043
Val - 18.314
NVa - 18.616
18.90919.10519.26119.437 19.865
Ile - 20.096
Leu - 20.317
Phe - 20.606
20.946
21.75521.849
21.970
AU
0.000
0.005
0.010
0.015
0.020
0.025
0.030
0.035
0.040
0.045
0.050
0.055
0.060
0.065
0.070
0.075
0.080
Minutes
1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00 7.50 8.00 8.50 9.00 9.50 10.00 10.50 11.00 11.50 12.00 12.50 13.00 13.50 14.00 14.50 15.00 15.50 16.00 16.50 17.00 17.50 18.00 18.50 19.00 19.50 20.00 20.50 21.00 21.50 22.00
AMINO-01 (FEBRUARY 2017) - APPENDICES
FOR ERP USE ONLY
DO NOT DISTRIBUTE