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666 

S

chneider

&

A

ndersen

:

J

ournal of

AOAC I

nternational

V

ol

. 98, N

o

. 3, 2015

Table 6. Residue identification summary

Analytes

identified, %,

n

= 28

Analyte Matrix

Concn of

analytes,

µg/kg

EU

a

FDA

b

Concn (>0.05 μg/kg) of

analytes in individual

blank samples

c

, μg/kg

MG Salmon Blank

7

7

0.10, 0.11

0.42

93

93

0.90

100 100

1.75

100 100

Incurred 100 100

Catfish Blank

0

0

0.42

96

100

0.90

93

93

1.75

100 100

Incurred

93

100

Shrimp Blank

4

4

0.42

100 100

0.90

100 100

1.75

93

93

Incurred

82

89

LMG Salmon Blank

4

4

0.08

0.42

100 100

0.90

100 100

1.75

100 100

Incurred 100 100

Catfish Blank

11

11

0.42

100 100

0.90

100 100

1.75

100 100

Incurred 100 100

Shrimp Blank

0

0

0.42

100 100

0.90

100 100

1.75

100 100

Incurred 100 100

CV Salmon Blank

57

57

0.14

0.42

100 100

0.90

100 100

1.75

100 100

Incurred

79

79

Catfish Blank

76

76

0.42

100 100

0.90

100 100

1.75

100 100

Table 6. (

continued

)

Analytes

identified, %,

n

= 28

Analyte Matrix

Concn of

analytes,

µg/kg

EU

a

FDA

b

Concn (>0.05 μg/kg) of

analytes in individual

blank samples

c

, μg/kg

Incurred

89

93

Shrimp Blank

46

46

0.30

0.42

100 100

0.90

100

96

1.75

100 100

Incurred 100 100

LCV Salmon Blank

50

43

0.06, 0.08

0.42

100

86

0.90

100 100

1.75

100 100

Incurred 100

96

Catfish Blank

33

22

0.08, 0.12, 0.13

0.42

100 100

0.90

96

96

1.75

100 100

Incurred

93

93

Shrimp Blank

0

0

0.42

93

93

0.90

93

86

1.75

93

89

Incurred

96

89

BG Salmon Blank

18

18

0.13

0.42

93

89

0.90

96

96

1.75

100 100

Incurred 100 100

Catfish Blank

15

15

0.08, 0.08

0.42

100 100

0.90

100 100

1.75

100 100

Incurred 100 100

Shrimp Blank

14

14

0.42

96

96

0.90

100 100

1.75

96

96

Incurred 100 100

a

 ±20–50% relative, based on value.

b

 ±10% absolute.

c

 Only blank samples that meet confirmation criteria for the analyte/matrix

pair and have a calculated concentration >0.05 μg/kg are reported.