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SRM 3264

St. John’s Wort Methanol Extract

Measured chlorogenic acid, flavonoids, and naphthodianthrones by LC with absorbance and

fluorescence detection.

SRM 3276

Carrot Extract in Oil (TPL/TC)

SRM 3277

Krill Oil

Coordinated measurement of fatty acids and astaxanthin through Grocery Manufacturer’s

Association.

SRM 3278

Tocopherols in Edible Oils (TPL/TC)

Extended certification range based on stability data.

SRM 3281

Cranberry (Fruit)

Measured organic acids by ID-LC-MS and ID-GC-MS. Method developed for measurement of

anthocyanidins and flavonols by LC-Abs. Method developed for measurement of anthocyanins

by LC-Abs. Method developed for fingerprinting of proanthocyanidins by LC-FL-MS.

Conducted stability testing of organic acids by LC-MS.

SRM 3282

Low-Calorie Cranberry Juice Cocktail

Measured organic acids by IC-CD and LC-UV, method developed for measurement of

anthocyanidins and flavonols by LC-Abs. Conducted stability testing of organic acids by LC-

MS.

SRM 3283

Cranberry Extract

Measured organic acids by IC-CD and ID-LC-MS, method developed for measurement of

anthocyanidins and flavonols by LC-Abs. Method developed for measurement of anthocyanins

by LC-Abs. Method developed for fingerprinting of proanthocyanidins by LC-FL-MS.

Conducted stability testing of organic acids by LC-MS.

SRM 3284

Cranberry-Containing Solid Oral Dosage Form

Measured organic acids by IC-CD and ID-LC-MS, method developed for measurement of

anthocyanidins and flavonols by LC-Abs. Method developed for measurement of anthocyanins

by LC-Abs. Method developed for fingerprinting of proanthocyanidins by LC-FL-MS.

Conducted stability testing of organic acids by LC-MS.

SRM 3285

Mixed Berry-Containing Solid Oral Dosage Form

Measured organic acids by IC-CD and ID-LC-MS, method developed for measurement of

anthocyanidins and flavonols by LC-Abs. Method developed for measurement of anthocyanins

by LC-Abs. Method developed for fingerprinting of proanthocyanidins by LC-FL-MS.

Conducted stability testing of organic acids by LC-MS.

SRM 3286

Organic Acids Calibration Solution (TPL/TC)

Prepared and measured organic acids by LC-UV. Drafted and finalized Certificate of Analysis.

Conducted stability testing of organic acids by LC-MS.

SRM 3287

Blueberry (Fruit)

Measured organic acids by IC-CD and ID-LC-MS, method developed for measurement of

anthocyanidins and flavonols by LC-Abs. Method developed for measurement of anthocyanins

by LC-Abs. Method developed for fingerprinting of proanthocyanidins by LC-FL-MS.

Measured water-soluble vitamins by ID-LC-MS. Conducted stability testing of organic acids by

LC-MS.

SRM 3290

Dry Cat Food (TPL/TC)

Measured water-soluble vitamins by ID-LC/MS/MS. Measured choline and carnitine by ID-LC-

MS (via Grace Hahm, student intern). Coordinated measurement of total nutrients, gravimetric

fat, and crude fiber through Grocery Manufacturer’s Association. Collected final data and

AOAC OMB Meeting Book

94