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prepared Report of Analysis summary for total nutrients. Prepared data for submission to SED.

Drafted and finalized Certificate of Analysis.

SRM 3291

Bilberry Extract

Measured organic acids by ID-LC-MS, method developed for measurement of organic acids by

IC-CD and of anthocyanidins and flavonols by LC-Abs. Method developed for measurement of

anthocyanins by LC-Abs. Method developed for fingerprinting of proanthocyanidins by LC-FL-

MS. Conducted stability testing of organic acids by LC-MS.

SRM 3951

Vitamin B

12

in Frozen Human Serum

Attempted to develop an ID-LC-MS/MS method for cyanocobalamin. Detection limits are not

low enough for the SRM.

AOAC OMB Meeting Book

95