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Multi Laboratory Test – AOAC First Action Method 2012.22 Ascorbic Acid (Vitamin C) in Infant Formula and

Adult/Pediatric Nutritionals.

RDLS-RD150006

E. Campos Giménez (NRC, Lausanne)

Page 26

CONFIDENTIAL

The contents of this document constitute a trade secret and the intellectual property rights thereto belong to Nestlé S. A., Vevey, Switzerland.

This document may not be reproduced or disclosed to third parties without prior authorisation.

Annex F: Reporting templates,

Continued

MLT samples

Concentration (ng/mL)

Calib level 1

Slope:

Calib level 2

Intercept:

Calib level 3

Calib level 4

Calib level 5

Calib level 6

Calib level 7

Concentration (ng/mL)

Calib level 1

Slope:

Calib level 2

Intercept:

Calib level 3

Calib level 4

Calib level 5

Calib level 6

Calib level 7

Calibration curve DAY 2

Peak Area

Ascorbic acid

Regression parameters

Regression parameters

Peak Area

Vitamin C (ascorbic acid) in Infant Formula and Adult/Pediatric Nutritional Formula by UHPLC-UV

AOAC First Action 2012.22: Multi-Laboratory Study

Name:

Compagny/Institution:

Country:

Calibration curve DAY 1

Ascorbic acid

Name:

Laboratory:

Country:

Extraction

Sample (g)

Water (g)

Mass (g)

Peak Area Results (mg/100 g)

Code

m1

m2

m Ascorbic acid Ascorbic acid

MLT Sample 1

VFJL091 not applicable not applicable

MLT Sample 2

EKVJ578

MLT Sample 3

GEUH577

MLT Sample 4

GLVC238

MLT Sample 5

LARU224

MLT Sample 6

VJKY373

MLT Sample 7

EPXW887

MLT Sample 8

GLBW236

MLT Sample 9

MNGN284

MLT Sample 10

YATV077 not applicable not applicable

MLT Sample 11

MOPG098 not applicable not applicable

MLT Sample 12

SNPZ056

MLT Sample 13

LKAU043 not applicable not applicable

MLT Sample 14

FHTX798

MLT Sample 15

FRZK569

MLT Sample 16

ADVZ021

MLT Sample 17

SJLQ035 not applicable not applicable

MLT Sample 18

LUJP087

MLT Sample 19

LHTK069 not applicable not applicable

MLT Sample 20

CBNJ010

Vitamin C (ascorbic acid) in Infant Formula and Adult/Pediatric Nutritional Formula by UHPLC-UV

AOAC First Action 2012.22: Multi-Laboratory Study

Day 2

Day 1

Sample reconstitution

Practice samples results

AOAC OMB Meeting Book

360