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Multi Laboratory Test – AOAC First Action Method 2012.22 Ascorbic Acid (Vitamin C) in Infant Formula and

Adult/Pediatric Nutritionals.

RDLS-RD150006

E. Campos Giménez (NRC, Lausanne)

Page 27

CONFIDENTIAL

The contents of this document constitute a trade secret and the intellectual property rights thereto belong to Nestlé S. A., Vevey, Switzerland.

This document may not be reproduced or disclosed to third parties without prior authorisation.

Annex G: Raw data practice samples

Raw data

practice

samples

Laboratory Practice sample 1: code YKLP059

Practice sample 2: code EPXW887

Code

Avg

CV

Avg

CV

1

12.0

11.7

11.8

2.4% 10.3

10.3

10.3

0.2%

2

11.0

10.9

11.0

0.9% 9.8

9.7

9.7

0.9%

3

11.6

11.2

11.4

3.5% 10.0

10.3

10.2

3.0%

4

11.4

11.0

11.2

3.7% 9.4

9.9

9.7

5.6%

5

10.6

10.6

10.6

0.1% 9.5

9.3

9.4

1.3%

6

11.2

11.4

11.3

1.5% 10.6

11.0

10.8

3.7%

7

12.7

12.8

12.8

0.8% 10.8

10.7

10.8

0.9%

8

14.5

14.5

14.5

0.4% 13.0

13.1

13.1

0.5%

9

11.6

11.3

11.5

2.6% 10.9

10.6

10.8

2.8%

10

12.2

12.1

12.1

1.2% 10.7

10.9

10.8

2.5%

11

12.6

12.6

12.6

0.1% 11.3

11.3

11.3

0.2%

12

12.5

12.5

12.5

0.5% 10.8

10.8

10.765

0.3%

13

10.3

10.2

10.2

1.0% 8.2

8.1

8.2

0.9%

14

11.2

11.1

11.2

0.7% 9.0

8.9

8.9

0.3%

15

14.7

14.4

14.5

2.7% 12.2

12.3

12.3

0.9%

16

13.4

13.3

13.4

0.7% 12.1

12.4

12.3

2.4%

17

12.3

12.2

12.2

0.8% 11.0

11.1

11.0

1.1%

18

12.0

11.8

11.9

1.7% 11.0

10.9

11.0

0.9%

19

11.4

11.2

11.3

1.5% 10.4

10.3

10.3

0.8%

20

21

11.4

11.3

11.4

0.9% 9.0

9.1

9.1

0.4%

22

11.3

10.6

23

11.5

11.6

11.5

0.5% 10.5

10.4

10.5

0.7%

24

11.5

12.2

11.9

5.7% 10.0

10.4

10.2

3.6%

Average

11.9

Average

10.5

SD

b

1.11

SD

b

1.14

S

r

0.167

S

r

0.149

RSD

r

1.4%

RSD

r

1.4%

S

R

1.115

S

R

1.142

RSD

R

9.3%

RSD

R

9.6%

Not analysed

AOAC OMB Meeting Book

361