16 / 97
Appendix 1: Linearity
Carnitine:
Actual
Concentration
(ng/g)
IS Actual
Concentration
(ng/g)
Area
(counts)
IS Area
(counts)
Concentration
ratio
Area ratio
std 1
4,6129
217,8116
3329,5
160220,7
0,021178395 0,020780686
std 2
9,0881
225,4382
7139,4
181885,2
0,040313044 0,039252491
std 3
38,1799
209,5343
29263,0 166593,2
0,182213127 0,175655523
std 4
74,0862
221,8754
55518,4 170267,0
0,333909032 0,326066704
std 5
146,2597
223,4094
112370,8 169939,0
0,6546712
0,661242287
std 6
256,4854
218,8944
183940,7 162286,4
1,171731209 1,13343267
std 7
550,7591
222,5433
363396,5 157346,8
2,474840177 2,309526344
std 8
1000,0994
221,0921
611060,3 140867,3
4,523451539 4,337842857
std 9
1550,7960
221,9617
807552,3 120998,7
6,986772943 6,674058219
std 1
4,6129
217,8116
3769,3
165826,3
0,021178395 0,022730696
std 2
9,0881
225,4382
6802,4
178225,4
0,040313044 0,038167521
std 3
38,1799
209,5343
30022,4 168285,8
0,182213127 0,178401211
std 4
74,0862
221,8754
55438,6 170807,8
0,333909032 0,324567286
std 5
146,2597
223,4094
111210,2 175511,7
0,6546712
0,633634036
std 6
256,4854
218,8944
188626,3 164762,3
1,171731209 1,144839091
std 7
550,7591
222,5433
354499,4 149704,4
2,474840177 2,367995416
std 8
1000,0994
221,0921
612058,0 138066,6
4,523451539 4,433062372
std 9
1550,7960
221,9617
892823,7 132958,5
6,986772943 6,715054693
SUMMARY OUTPUT
Regression Statistics
Multiple R
0,999913128
R Square
0,999826263
Adjusted R Square 0,999815404
Standard Error
0,030825052
Observations
18
ANAVA
df
SS
MS
F
Significance F
Regression 1 87,49023889 87,49023889 92077,17128 1,63032E-31
Residual
16 0,015202941 0,000950184
Total
17 87,50544183
Coefficients
Std. Error
t Stat
P-value
Lower 95%
Upper 95%
Intercept
0,00455914 0,009271008 0,491763144 0,629565074 -0,01509451 0,024212798
Concentration ratio 0,959609823 0,003162414 303,4422042 1,63032E-31 0,95290580 0,966313841
RESIDUAL OUTPUT
Observation Predicted Area
Residuals
1
0,024882135 -0,004101449
2
0,043243933 -0,003991442
3
0,179412646 -0,003757124
4
0,324981527 0,001085177
5
0,632788054 0,028454233
6
1,128963918 0,004468752
7
2,379440084 -0,069913739
8
4,345307669 -0,007464813
Carn-06 - Validation Report
FOR ERP USE ONLY
DO NOT DISTRIBUTE