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day 15

338,625

342,389

day 15

2 681,014 340,507

7,083848

day 16

332,365

340,596

day 16

2 672,961 336,4805 33,8746805

Average of all days

347,38 mg/kg

ANAVA

Source of Variation

SS

df

MS

F

P-value

F crit

Between Groups

3354,811135 15 223,6540757 5,188242953 0,001098565 2,352222763

Within Groups

689,7258365 16 43,10786478

Total

4044,536971 31

Appendix 3: Limit of detection / quantification

Carnitine:

Replicate

9,414 ng/g

9,379 ng/g

9,145 ng/g

9,247 ng/g

9,418 ng/g

9,896 ng/g

9,409 ng/g

9,432 ng/g

9,810 ng/g

10,080 ng/g

Mean 9,523 ng/g

Std

0,301 ng/g

LOD 0,9 ng/g

LOQ 3,0 ng/g

In samples

LOD 124 ng/g = 0,1 µg/g

LOQ 413 ng/g = 0,4 µg/g

Carn-06 - Validation Report

FOR ERP USE ONLY

DO NOT DISTRIBUTE