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Table 2014.2A (cont’d)

: Comparative Results for the Detection of

Listeria

in Full Fat Cottage Cheese (4% Milk Fat) by the 3M

MDA

Listeria

Method vs.

1

AOAC OMA 993.12 in a Collaborative Study (High Level)

2

Statistic

MPN/

Test Portion Laboratory

Candidate

presumptive (CP)

Candidate confirmed

(CC)

Candidate result (C)

Reference method

(R)

C vs. R

N

X

POD(CP)

N

X

POD(CC)

N

X

POD(C) N

X POD(R) dLPOD

(C,R)

dLPOD

(CP,CC)

4.83

3.30

7.07

1

12

12

1.00

12

12

1.00

12

12

1.00

12

12

1.00

0.00

0.00

2

12

12

1.00

12

12

1.00

12

12

1.00

12

12

1.00

0.00

0.00

3

12

12

1.00

12

12

1.00

12

12

1.00

12

12

1.00

0.00

0.00

4

a

NA NA

NA

NA NA

NA

NA NA

NA

NA NA

NA

NA

NA

5

a

NA NA

NA

NA NA

NA

NA NA

NA

NA NA

NA

NA

NA

6

a

12

12

1.00

12

12

1.00

12

12

1.00

12

7

0.58

0.42

0.00

7

12

12

1.00

12

12

1.00

12

12

1.00

12

12

1.00

0.00

0.00

8

12

12

1.00

12

12

1.00

12

12

1.00

12

12

1.00

0.00

0.00

9

12

12

1.00

12

12

1.00

12

12

1.00

12

12

1.00

0.00

0.00

10

12

12

1.00

12

12

1.00

12

12

1.00

12

12

1.00

0.00

0.00

11

12

12

1.00

12

12

1.00

12

12

1.00

12

12

1.00

0.00

0.00

12

12

12

1.00

12

12

1.00

12

12

1.00

12

12

1.00

0.00

0.00

13

a

12

2

0.17

12

2

0.17

12

12

1.00

12

12

1.00

-0.83

0.00

14

12

12

1.00

12

12

1.00

12

12

1.00

12

12

1.00

0.00

0.00

15

12

12

1.00

12

12

1.00

12

12

1.00

12

12

1.00

0.00

0.00

Estimate

All

132 132

1.00

132 132

1.00

132 132

1.00

132 132

1.00

0.00

0.00

LCL

0.97

0.97

0.97

0.97

-0.03

-0.03

UCL

1.00

1.00

1.00

1.00

0.03

0.03

s

r

b

0.00

0.00

0.00

0.00

LCL

0.00

0.00

0.00

0.00

UCL

0.16

0.16

0.16

0.16

s

L

c

0.00

0.00

0.00

0.00

LCL

0.00

0.00

0.00

0.00

UCL

0.16

0.16

0.16

0.16

s

R

d

0.00

0.00

0.00

0.00

UCL

0.00

0.00

0.00

0.00

LCL

0.23

0.23

0.23

0.23

P

T

e

1.0000

1.0000

1.0000

1.0000

a

Results were not used in statistical analysis due to deviation from testing protocol.

3

c

Repeatability Standard Deviation,

d

Among-Laboratory Standard Deviation,

e

Reproducibility Standard Deviation,

f

P

T

Value =Homogeneity test of laboratory PODs

4

LCL – Lower Confidence Limit; UCL – Upper Confidence Limit;

NA- laboratory results were not received

5

6

7

8

Candidates for 2016 Method of the Year

132