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M
astovska
et al
.
:
J
ournal of
AOAC I
nternational
V
ol
. 98, N
o
. 2, 2015
Table 12. Recoveries (%) of the studied PAHs in oyster obtained by a collaborator storing the test samples SFC O1–O7 at
–20°C
PAH
SFC O1
SFC O2
SFC O3
SFC O4
SFC O5
SFC O6
SFC O7
Mean
RSD, %
1,7-DMP
93
95
93
102
90
107
92
96
6.3
1-MN
102
102
98
124
98
111
106
9.5
1-MP
97
99
100
93
109
94
99
5.8
2,6-DMN
85
77
91
65
71
73
77
13
3-MC
92
94
98
96
97
96
95
2.1
Ant
41
47
51
50
53
44
48
9.6
BaA
74
75
80
78
81
76
77
3.5
BaP
47
51
56
52
54
50
52
6.3
BbF
82
88
92
87
89
86
87
3.7
BghiP
87
83
87
82
84
90
86
3.4
BkF
86
85
92
89
89
88
88
2.9
Chr
86
85
91
87
88
87
87
2.5
DBahA
87
84
89
82
84
86
85
2.7
Fln
86
86
93
83
77
86
85
6.3
Flt
85
84
90
87
88
91
87
3.2
IcdP
88
85
88
86
86
89
87
1.6
Naph
93
93
101
95
92
94
95
3.4
Phe
89
87
93
90
89
88
89
2.2
Pyr
86
85
89
88
88
85
87
2.2
Table 13. Recoveries (%) of the studied PAHs in oyster obtained bya collaborator storing the test samples SFC O1–O7 at
–70°C
PAH
SFC O1 SFC O2 SFC O3 SFC O4 SFC O5 SFC O6 SFC O7 Mean RSD, %
1,7-DMP
94
99
108
95
98
106
96
100
5.4
1-MN
107
109
109
110
101
101
106
3.8
1-MP
94
100
100
92
102
88
96
5.5
2,6-DMN
85
90
89
80
77
78
83
6.8
3-MC
99
101
102
96
100
93
99
3.5
Ant
92
91
89
87
91
84
89
3.3
BaA
88
90
90
87
91
81
88
4.0
BaP
90
87
86
85
88
82
86
3.0
BbF
90
93
93
87
92
83
90
4.2
BghiP
94
95
94
89
94
90
93
2.7
BkF
91
92
91
90
94
85
90
3.1
Chr
90
92
92
88
93
84
90
3.8
DBahA
95
96
95
92
96
89
94
3.1
Fln
93
94
93
88
92
87
91
3.2
Flt
95
92
94
88
92
86
91
4.1
IcdP
94
93
93
87
92
87
91
3.5
Naph
94
99
96
93
96
88
94
3.8
Phe
90
92
91
89
93
84
90
3.6
Pyr
92
94
93
90
94
86
91
3.3
Candidates for 2016 Method of the Year
257