AOAC SPIFAN ERP Meeting Book (3-16-16)

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Fonterra Co-operative Group
Page 26
Table D9: Data vitamin D 3 100% recovery experiment 2
Sample Units
Vitamin D2 (μg hg-1 )
Recovery
(%) Unspiked
sample
Spiked
sample Spike
Child Formula Powder μg hg-1 0.0 10.2 10.0 101.8
Infant Elemental Powder μg hg-1 0.0 9.9 10.0 98.8
Adult Nutritional RTF High Protein μg L -1 0.0 19.7 20.0 98.3
Adult Nutritional RTF High Fat μg L -1 0.0 20.0 20.0 99.9
Infant Formula RTF, Milk-Based μg L -1 0.0 19.7 20.0 98.5
Table D10: Data vitamin D3 50% recovery experiment 2
Sample Units
Vitamin D2 (μg hg-1 )
Recovery
(%) Unspiked
sample
Spiked
sample Spike
Child Formula Powder μg hg-1 0.0 5.0 4.9 101.5
Infant Elemental Powder μg hg-1 0.0 4.8 4.9 96.9
Adult Nutritional RTF High Protein μg L -1 0.0 9.6 9.8 98.0
Adult Nutritional RTF High Fat μg L -1 0.0 10.2 9.8 104.1
Infant Formula RTF, Milk-Based μg L -1 0.0 9.2 9.8 93.9
Table D11: Data vitamin D3 100% recovery experiment 3
Sample Units
Vitamin D2 (μg hg-1 )
Recovery
(%) Unspiked
sample
Spiked
sample Spike
Child Formula Powder μg hg-1 0.0 10.1 9.9 101.5
Infant Elemental Powder μg hg-1 0.0 9.8 9.9 98.7
Adult Nutritional RTF High Protein μg L -1 0.0 19.5 19.9 98.2
Adult Nutritional RTF High Fat μg L -1 0.0 19.9 19.9 100.1
Infant Formula RTF, Milk-Based μg L -1 0.0 19.3 19.9 97.4
Table D12: Data vitamin D3 50% recovery experiment 3
Sample Units
Vitamin D2 (μg hg-1 )
Recovery
(%) Unspiked
sample
Spiked
sample Spike
Child Formula Powder μg hg-1 0.0 5.0 4.9 101.5
Infant Elemental Powder μg hg-1 0.0 4.7 4.9 95.4
Adult Nutritional RTF High Protein μg L -1 0.0 9.6 9.7 98.7
Adult Nutritional RTF High Fat μg L -1 0.0 10.1 9.7 103.3
Infant Formula RTF, Milk-Based μg L -1 0.0 9.1 9.7 93.8
VitD-18 (February 2016)
FOR ERP USE ONLY
DO NOT DISTRIBUTE