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AOAC SPIFAN ERP MEETING BOOK COVER
1

FIRST ACTION/METHOD EVALUATION FORM/VALIDATION DATA
2

AMINO ACIDS
3

Amino Acids SMPR
3

Amino-03
7

Amino-03 - Method (UHPLC)
7

Amino-03 - Acids Hydrolysis Calibration Table/Report
16

Amino-03 - Alkaline Hydrolysis Calibration Table/Report
61

Amino-03 - Oxidatives Hydrolysis Calibration Table/Report
70

BIOTIN
83

Biotin SMPR
83

Bio-02
85

Bio-02 - Appendix 1
85

Bio-02 - Validation Report
89

Bio-02 - Appendices 2 - 6
98

Bio-03
103

Bio-03 - Method
103

Bio-03 - Appendix A
113

Bio-03 - SLV
115

Bio-03 - Tables
119

Bio-03 - Chromatography
122

Bio-03 - Journal Article
129

Bio-03 - Method Evaluation Form
133

B VITAMINS
141

B Vitamins SMPR (1,2,3,6)
141

BVit-02
145

BVit-03
146

BVit-03 - Method
146

BVit-03 - (WSV VAL Linearity) Summary Report
179

BVit-03 - (WSV VAL Linearity) Calibration Report
183

BVit-03 - (WSV VAL Linearity) Sample Report
188

BVit-03 - (WSV VAL P&A) Summary Report
231

BVit-03 - (WSV VAL P&A) Calibration Report
235

BVit-03 - (WSV VAL P&A) Sample Report
241

BVit-03 - (WSV-SRM) Summary Report
308

BVit-03 - (WSV-SRM) Calibration Report
312

BVit-03 - (WSV-SRM) Sample Report
316

CAROTENOIDS
367

Carotenoids SMPR
367

Carot-01
369

Carot-01 - Tables
372

Carot-02
375

Carot-02 - Method
375

Carot-02 - Chromatograms
382

Carot-02 - Tables
385

CHLORIDE
387

Chloride SMPR
387

Combined Chloride Method (2015.07/2015.08)
389

2015.07/2015.08 (Chlor-02/Chlor-04)
389

2015.07/2015.08 - Figures 1 & 2
397

*Chlor-03/Fluor-02
399

Chlor-03/Fluor-02 - SLV
399

Chlor-03/Fluor-02 - Table 1
405

Chlor-03/Fluor-02 - Figure 1 Chromatography
406

Chlor-03/Fluor-02 - Table 2-7
407

Chlor-03/Fluor-02 - MEF
413

CHOLINE
419

Choline SMPR
419

Chol-08/Carn-07 (2015.10)
421

Chol-08 - Method
421

Chol-08 - SLV
431

Chol-08 - Tables 1-3
433

Chol-08 - Validation Results - Tables 4-9
435

Chol-08 - LOQ - Tables 10-15
440

Chol-08 - Accuracy/Recovery - Tables 16-23
444

Chol-08 - NIST SRM - Tables 24-27
452

Chol-08 - References
454

FLUORIDE
457

Fluoride SMPR
457

*Fluor-02/Chlor-03
459

Fluor-02/Chlor-03 - SLV
459

Fluor-02/Chlor-03 - Table 1
465

Fluor-02/Chlor-03 - Figure 1 Chromatography
466

Fluor-02/Chlor-03 - Table 2-7
467

Fluor-02/Chlor-03 - MEF
473

FOLATE
479

Folate SMPR
479

Fol-20
481

Fol-20 - Method
481

Fol-20 - Results Table 1-3/Appendix Table 1
488

2013.13 (Fol-21) - NOTES
491

2011.06 (Fol-22)
505

2011.06 (Fol-22) - Method
505

2011.06 (Fol-22) - Results-Table 1
509

2011.06 (Fol-22) - Tables 2-3
511

2011.06 (Fol-22) - Figure 1/Table-4
514

2011.06 (Fol-22) - Figure 2/Table-5
515

2011.06 (Fol-22) - Table-6
516

2011.06 (Fol-22) - Figure 3-5
517

2011.06 (Fol-22) - Table 7-13
520

2011.06 (Fol-22) - Analysis of SPIFAN Matrices-Tables 14-17
524

2011.06 (Fol-22) - Folate Analysis-Table 18-22
531

2011.06 (Fol-22) - LOD/LOQ
537

2011.06 (Fol-22) - Conclusions
538

FRUCTANS (FOS)
541

Fructans (FOS) SMPR
541

Fos-01
543

Fos-01 - SLV
544

Fos-01 - Annex 1 - Chromatogram
556

Fos-01 - Annex 2 - Calibration Curve (Fructose/Sucrose)
557

Fos-01 - Annex 3 - Chromatogram (J4G0975 Sample)
558

Fos-01 - Annex 4 - Results for the Precision
559

Fos-01 - Annex 5 - Results for the Recovery
560

Fos-01 - MEF
561

Fos-04
571

Fos-04 - Method-Part 1
571

Fos-04 - Part 2
575

Fos-04 - Tables & Figures
576

Fos-04 - Appendix A (Figures/Chromatograms)
587

Fos-04 - Appendix B (Figures/Chromatograms)
599

Fos-04 - Appendix C (Table C-1)
609

Fos-04 - MEF
611

VITAMIN D
617

Vitamin D SMPR
617

VitD-17
619

VitD-17 - Method & Tables 1-7
619

VitD-17 - MEF
625

VitD-18
635

VitD-18 - Method
635

VitD-18 - Validation
645

VitD-18 - Tables 1-4/Figures 1-6
649

VitD-18 - Precision-Table 5
652

VitD-18 - LOQ/LOD-Table 6-7
654

VitD-18 - Recovery-Table 8-11
655

VitD-18 - Bias against SRM-Table 12
657

VitD-18 - Bias against Ref.Method-Table 13
658

VitD-18 - Chromatography
659

VitD-18 - References
661

VitD-18 - Appendices
662

VitD-18 - Appendix A
662

VitD-18 - Appendix B
664

VitD-18 - Appendix C
667

VitD-18 - Appendix D
668

VitD-18 - Appendix E
671

VitD-18 - Appendix F
672

VitD-18 - Appendix G
674

VitD-18 - MEF
675

FINAL ACTION
680

Vitamin C SMPR
681

2012.22 (VitC-03) MLT
683

Additional Data
687

Background
688

Experimental
689

Results & Conclusion
690

Conclusion
692

ANNEX A: List of Participants
694

ANNEX B: Raw Data
695