AOAC SPIFAN ERP Meeting Book (3-16-16)

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Table 3: Precision—Repeatability and intermediate precision
Child Formula Powder 00847RF00 3 1.2 μg hg -1 RTF – 5.4% 0.12 μg hg -1 RTF ≤15
Infant Elemental Powder 00796RF 3 1.1 μg hg -1 RTF – 5.4% 1.5 μg hg -1 RTF
Adult Nutritional RTF High Protein 00821RF00 3 1 μg hg-1 RTF – 7.4% 2.5 μg hg -1 RTF
Adult Nutritional RTF High Fat 00820RF00 3 0.9 μg hg -1 RTF – 5.0% 5.1 μg hg -1 RTF
Infant Formula RTF, Milk-Based EV4H2Q 3 0.9 μg hg -1 RTF – 4.4%
In-House Reference IF Powder — 12 1.2 μg hg -1 RTF 5.2% 5.4%
NIST SRM1849a CLC10-b 12 1.1 μg hg -1 RTF 2.8% 5.4%
IF Powder Part. Hydrolysed Milk-Based 410057652Z 12 1 μg hg-1 RTF 4.4% 7.4%
IF Powder Part. Hydrolysed Soy-Based 410457651Z 12 0.9 μg hg -1 RTF 1.8% 5.0%
Toddler Formula Powder Milk-Based 4052755861 12 0.9 μg hg -1 RTF 2.2% 4.4%
Infant Formula Powder Milk-Based 4044755861 12 0.9 μg hg -1 RTF 2.1% 4.4%
Adult Nutritional Powder Low Fat 00859RF00 12 0.4 μg hg -1 RTF 3.7% 6.3%
Child Formula Powder 00866RF00 12 0.9 μg hg -1 RTF 3.3% 5.8%
Infant Elemental Powder 00795RF 12 0.9 μg hg -1 RTF 3.5% 3.1%
Infant Formula Powder FOS/GOS-Based 50350017W1 12 0.8 μg hg -1 RTF 1.5% 4.7%
Infant Formula Powder Milk-Based K16NTAV 12 1.1 μg hg -1 RTF 3.3% 6.4%
Infant Formula Powder Soy-Based E10NWZC 12 1.1 μg hg -1 RTF 2.6% 3.6%
Infant Formula RTF Milk-Based EV4H2R 12 0.7 μg hg -1 RTF 2.3% 7.8%
Adult Nutritional RTF High Protein 00730RF00 12 1 μg hg-1 RTF 1.6% 5.2%
Adult Nutritional RTF High Fat 00729RF00 12 1.3 μg hg -1 RTF 4.9% 7.9%
Footnotes: Global Mean % 3.0% 5.0%
(1) Estimated from spiked recovery study, intermediate precision only, no repeability data available
Product SPIFAN Code Analyte Replicates
(n) Conc. Level
Vitamin D3
Vitamin D2
(1)
RSDr RSDiR Concentration
≤11
Vitamin D No limit set
RSDr RSDiR
SMPR
Requirements
SPIFAN ERP X Checklist v 1.0
VitD-18 (February 2016)
FOR ERP USE ONLY
DO NOT DISTRIBUTE