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SPIFAN Expert Review Panel Report
March 19, 2014
Final
Vitamin A
2011.07 - Vitamin A in Infant
Formula and Adult Nutritionals
UPLC-UV
Don Gilliland
Jinchuan Yang
*Motion to keep method
Yes- 11/ No-0 /Abstain-1
◊
Keep method
◊
Desire for combo method
◊
Has SLV data, but not published
2011.15 - Vitamin A (Retinol) in
Infant Formula and Adult
Nutritionals Liquid Chromatography
Sneh Bhandari
Adrienne McMahon
*Motion to repeal
Yes- 11/ No-0 /Abstain-1
◊
Vitamin D
2011.12 - Vitamins D
2
and D
3
in
Infant Formula and Adult
Nutritionals Ultra Pressure Liquid
Chromatography with Mass
Spectrometry Detection (UPLC-
MS/MS)
Brendon Gill
Adrienne McMahon
*Motion to repeal
Yes- 10/ No-0 /Abstain-1
2011.13 - Vitamins D
2
and D
3
in
Infant Formula and Adult
Nutritionals LC-MS/MS
Matt Sliva for Scott
Christiansen
Shay Phillips
*Motion to repeal
Yes- 9/ No-0 /Abstain-1
◊
Original method was withdrawn
and resubmitted
◊
Vitamin B12
2011.08 - Improved AOAC First
Action 2011.08 for the analysis of
vitamin B
12
in Infant Formula and
Adult/Pediatric Formulas. Single
Laboratory Validation
(Modification)
Bill Mindak
Matt Sliva for Scott
Christiansen
Brendon Gill
Shay Phillips
*Motion to give the
method a new number
(TBD)
Yes- 11/ No-0 /Abstain-1
*Motion to repeal old
number (2011.08)
Yes- 10/ No-0 /Abstain-1
◊
Keep or give it a new number?
◊
Reference back to the old
number from the AOAC Journal
◊
See section 4 for additional
comments
2011.09 - Vitamin B
12
in Infant
Formula and Adult Nutritionals HPLC
After Purification on an
Immunoafïnity Column
Matt Sliva for Scott
Christiansen
Estela Kneeteman
*Motion to keep
Yes- 11/ No-0 /Abstain-1
◊
Keep the method
2011.16 - Vitamin B
12
in Infant
Formula and Adult Nutritionals
Surface Plasmon Resonance
Shay Phillips
John Austad
*Motion to repeal
Yes- 10/ No-0 /Abstain-1
◊
VII.
DISCUSS REQUIREMENTS/EXPECTATIONS RELATED TO MULTI-LABORATORY TESTING REPORTS, AN
UPDATE ON MULTI-LABORATORY TESTING AND SCHEDULE
Robert Rankin (International Formula Council) discussed the template to be used for Multi-Laboratory Testing
(MLT) reports; the reports will be in a standardized format. The draft template and will be available soon, it’s
currently in review with the Methods Committee on Statistics.
VIII.
UPCOMING METHOD AUTHOR ORIENTATION
Deborah McKenzie, AOAC provided an overview of the upcoming method author orientation including
requirements for submission of Multi-Laboratory Testing (MLT) reports.
IX.
NEXT STEPS/FEEDBACK FROM ERP
Darryl Sullivan provided next steps including deadline dates. The study directors will need to complete the
evaluation sheets and the ERP may have seven (7) MLT reports for review with a mid-July deadline, while
providing the ERP with four (4) weeks to complete a thorough review. AOAC will need to be informed if ERP
members will be unable to attend the AOAC Annual Meeting in Boca Raton, FL. No feedback/comments were
received from the ERP pertaining to the meeting.
ERP PROFILE SUMMARIES
29