74-75 / 328
•
Investigate a better baseline
separation for Peak 1
•
pH of phosphate buffer
•
Column temperature
•
Heat stability during the
extraction
•
Simplify the preparation of the
extract products
•
Limit number of reference
standards to one withanolide and
one withanoside with use of
response factors
•
Provide data on finished products
•
When specifying columns put “or
equivalent.”
•
Clarify the discard volume in the
filtration step
•
Provide data on method LOQ
ACTION ITEMS:
1.
Staff: Send notification to method author, requesting MS Word copy of method/manuscript for publication. Send follow up documentation on
requirements and ERP recommendations for Final Action Official Methods status consideration.
II.
Folin C
Folin C ERP Members Present:
Darryl Sullivan, Covance (Chair); Nour Eddine Es-Safi, Mohammad V University in Rabat; Martha Jennens, Covance; Dana
Krueger, Krueger Food Laboratories; Tom Phillips, State of MD; Catherine Rimmer, NIST; Aniko Solyom, GAAS Analytical; John Spzylka,
Mérieux
Nutrisciences;
Joseph Zhou, Sunshineville Health Products
Folin C ERP Members Absent:
John Finley, LSU (Retired), Prashant Ingle, Herbalife; Jungmin Lee, USDA
AOAC Method #
Manuscript Title
ERP Decisions
Consensus
Decision Date
FOL-01
Folin-Ciocalteau Reagent for
The ERP agreed not to take action on this
No motion made.
December 10, 2015
ERP PROFILE SUMMARIES
64