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in the nonspiked sample in micrograms per kg. ρ
Spiked
is the
concentration of sodium fluoroacetate spiked in the sample in
micrograms per kg (calculated value).
The recovery rate should be between 70–120% when spiked
at the 1 µg/kg level.
References
(1) Commission Decision 2002/657/EC of 12 August
2002 implementing Council Directive 96/23/EC
concerning the performance of analytical methods and
the interpretation of results,
Off. J. Eur. Commun.
(2002)
L221
, 8–36.
http://eur-lex.europa.eu/legal-content/EN/TXT/F/?uri=CELEX:32002D0657&rid=1
(2) SANCO/12571/2013: Guidance document on analytical quality
control and validation procedures for pesticide residues analysis
in food and feed,
http://ec.europa.eu/food/plant/pesticides/guidance_documents/docs/qualcontrol_en.pdf
(3) AOAC SMPR
2015.001
J. AOAC Int
. (future issue)
253