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1134 

Mottier et al.

: J

ournal of

AOAC I

nternational

Vol. 98, No. 4, 2015

in the nonspiked sample in micrograms per kg. ρ

Spiked

is the

concentration of sodium fluoroacetate spiked in the sample in

micrograms per kg (calculated value).

The recovery rate should be between 70–120% when spiked

at the 1 µg/kg level.

References

 (1) Commission Decision 2002/657/EC of 12 August

2002 implementing Council Directive 96/23/EC

concerning the performance of analytical methods and

the interpretation of results,

Off. J. Eur. Commun.

(2002)

L221

, 8–36.

http://eur-lex.europa.eu/legal-content/EN/TXT/

F/?uri=CELEX:32002D0657&rid=1

 (2) SANCO/12571/2013: Guidance document on analytical quality

control and validation procedures for pesticide residues analysis

in food and feed,

http://ec.europa.eu/food/plant/pesticides/

guidance_documents/docs/qualcontrol_en.pdf

 (3) AOAC SMPR

2015.001

J. AOAC Int

. (future issue)

253