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AOAC RESEARCH INSTITUTE

AOAC

OFFICIAL METHODS OF ANALYSIS

(OMA)

OMAMAN-28/AOAC 2006.03

Study Director: Sharon Webb, University of Kentucky, Division of Regulatory Services,

103 Regulatory Services Bldg, Lexington , Kentucky 40546-0275

ER 8

At present, there are no safety concerns with the exception of the contemporary use of nitric

and hydrochloridric acids. In addition, the use of microwave digestion units at 200 °C has to be

carefully considered.

ER 9

I have not seen a review by the safety advisor. The safety checklist seems appropriate. I do not

have any additional concerns regarding the safety of this method.

ER 10

No cautions provided

Are there any concerns regarding the data manipulation, data tables, or statistical analysis?

ER 1

No concerns

ER 2

No

ER 3

unknown, no access to this

ER 4

No

ER 5

none

ER 6

no

ER 7

No

ER 8

At present, there are no concerns with relation to data manipulation, data tables and statistical

analysis.

ER 9

I have not seen a review by the statistical advisor. However I do not have any concerns

regarding the statistics used to support this method other than the use of a broader selection of

materials (organic derivation) used in future work or data reviews.

ER 10

None observed.

EDITORIAL EVALUATION CRITERIA

Is the Validation Study Manuscript in a format acceptable to AOAC?

ER 1

Yes

ER 2

Yes

ER 3

Yes

ER 4

Yes

ER 5

Yes

ER 6

Yes

ER 7

Yes

ER 8

Yes

ER 9

Yes

ER 10

Yes

Is the method described in sufficient detail so that it is relatively easy to understand, including equations and

procedures for calculation of results (are all terms explained)?

ER 1

Yes

ER 2

Yes

ER 3

Yes

ER 4

Yes

ER 5

Yes

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