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EuroWire – November 2010

50

Compounds & colourings

Melt temperature plays a critical role in the insulation phase of

medium voltage (MV), high voltage (HV) and extra high voltage

(EHV) XLPE insulated power cable extrusion, with organic

peroxides used for cross-linking with both insulation and

semi-conductive materials.

Acceptable extrudate temperature range is limited since proper

melting and homogeneity set the lower limit, while avoiding

premature cross-linking sets the upper limit.

Extrudate temperature can affect both quality of the cable

and the productivity. Premature cross-linking before or on the

screens creates pressure build-up in the extruder and reduces

running time. Premature cross-linking after screens, on the other

hand, may lead to ambers or scorch in the insulation itself.

In continuous vulcanizing (CV) lines the common practise is

either to use thermocouple sensors or to measure extrudate

temperature before start-up using a hand-held meter after

crosshead. Before the introduction of an extrudate temperature

gauge based on ultrasonic velocity there has not been an online

solution available that is both non-contact and reliable.

In the majority of cases extrusion lines are not equipped with an

online melt temperature measurement system to record and to

control plastic melt temperature during the extrusion process.

Normally this temperature is measured only during the

commissioning of the extrusion line at various line speeds and

pressure conditions or later, during servicing.

For this purpose various methods are employed, such as the use

of shielded thermocouples or infrared pyrometers, but each of

these methods has at least minor imperfections.

Using a thermocouple for contact, single-point measurement

has a relatively slow response time. If the thermocouple does not

penetrate into the melt, only the melt surface temperature or the

temperature of the metallic extruder flow channel is measured.

If the thermocouple penetrates into the melt shear heating

errors can occur, presenting a local increase of temperature.

Furthermore the thermocouple influences the melt flow

properties and premature cross-linking takes place.

Using an infrared pyrometer a contact-free temperature

measurement with an improved response time is possible

though, still, mainly the surface temperature of the PE melt is

measured because the penetration depth of infrared radiation

in LDPE (low density polyethylene) amounts to only several

millimetres. Furthermore the presence of specific fillers in the

PE melt can drastically decrease this penetration depth.

The ultrasonic velocity in plastic compounds strongly depends

on the temperature of the material. Therefore it is essential to

compensate this influence if, for example, the dimensions of

plastic insulated power cables (eg insulation wall thickness,

eccentricity) are measured using an ultrasonic technique. On

the other hand, a known temperature dependence of a material’s

ultrasonic velocity can be used to determine the material

temperature by measuring its ultrasonic velocity.

One of the challenges in the measurement of ultrasonic velo-

city in plastic melts is the high ultrasonic attenuation of these

materials.

Ultrasonic temperature

measurement system for

polyethylene melts

by Dr T Clausen of Sikora AG and Dr P Huotari of Maillefer Extrusion Oy

Schematic view of the adapter in the extrusion line

Adapter with measuring

gauge