Review Team (February 2016).pdf

peak noise between 6.0 and 7.0 min over five injections of a prepared sample. The estimated

LOD and LOQ for fluoride were 1.27 and 4.24

g/100g respectively. The estimated LOD and

LOQ for chloride were 0.006 and 0.02

g/100g respectively.

Summary

The accuracy data for fluoride and chloride met the criteria specified in the SMPR. The

limit of quantitation for fluoride was estimated to be 4.24

g/100g. The limit of detection was

estimated to be 1.27

g/100g. Acceptable linearity was demonstrated for both fluoride and

chloride over a range specified in SMPR.

This method is found to be suitable for the analysis of fluoride and chloride in a single

method for all SPIFAN matrices.

Fluor-02/Chlor-03 (February 2016)

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