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AOAC SPIFAN Review Team Book Cover
1

AMINO ACIDS
3

Amino Acids SMPR
3

Amino-03
7

Amino-03 - UHPLC
7

Amino-03 - Acids Hydrolysis Calibration Table/Report
16

Amino-03 - Alkaline Hydrolysis Calibration Table/Report
61

Amino-03 - Oxidatives Hydrolysis Calibration Table/Report
70

BIOTIN
82

Biotin SMPR
82

Bio-02
83

Bio-02 - Appendix 1
83

Bio-02 - Validation Report
87

Bio-02 - Appendices 2 - 6
96

Bio-03
101

Bio-03 - Method
101

Bio-03 - Appendix A
110

Bio-03 - SLV
113

Bio-03 - Tables
117

Bio-03 - Chromatography
120

Bio-03 - Journal Article
126

Bio-03 - Method Evaluation Form
130

B VITAMINS
137

B Vitamins SMPR (1,2,3,6)
137

BVit-02
141

BVit-03
142

BVit-03 - Method
142

BVit-03 - (WSV VAL Linearity) Summary Report
175

BVit-03 - (WSV VAL Linearity) Calibration Report
179

BVit-03 - (WSV VAL Linearity) Sample Report
184

BVit-03 - (WSV VAL P&A) Summary Report
227

BVit-03 - (WSV VAL P&A) Calibration Report
231

BVit-03 - (WSV VAL P&A) Sample Report
237

BVit-03 - (WSV SRM) Summary Report
304

BVit-03 - (WSV SRM) Calibration Report
308

BVit-03 - (WSV SRM) Sample Report
312

CAROTENOIDS
363

Carotenoids SMPR
363

Carot-01
365

Carot-01 - Tables
368

Carot-02
371

Carot-02 - Method
371

Carot-02 - Chromatograms
378

Carot-02 - Tables
381

CHLORIDE
383

Chloride SMPR
383

Combined Chloride Method (2015.07/2015.08)
385

2015.07/2015.08 (Chlor-02/Chlor-04)
385

2015.07/2015.08 - Figures 1 & 2
393

*Chlor-03/Fluor-02
395

Chlor-03/Fluor-02 - SLV
395

Chlor-03/Fluor-02 - Table 1
401

Chlor-03/Fluor-02 - Figure 1 Chromatography
402

Chlor-03/Fluor-02 - Table 2-7
403

Chlor-03/Fluor-02 - MEF
409

CHOLINE
415

Choline SMPR
415

Chol-08/Carn-07 (2015.10)
417

Chol-08 - Method
417

Chol-08 - SLV
427

Chol-08 - Tables 1-3
429

Chol-08 - Validation Results - Tables 4-9
431

Chol-08 - LOQ - Tables 10-15
436

Chol-08 - Accuracy/Recovery - Tables 16-23
440

Chol-08 - NIST SRM - Tables 24-27
448

Chol-08 - References
450

FLUORIDE
453

Fluoride SMPR
453

*Fluor-02/Chlor-03
455

Fluor-02/Chlor-03 - SLV
455

Fluor-02/Chlor-03 - Table 1
461

Fluor-02/Chlor-03 - Figure 1 Chromatography
462

Fluor-02/Chlor-03 - Table 2-7
463

Fluor-02/Chlor-03 - MEF
469

FOLATE
475

Folate SMPR
475

Fol-20
477

Fol-20 - Method
477

Fol-20 - Results Table 1-3/Appendix Table 1
484

2013.13 (Fol-21) - NOTES
487

2011.06 (Fol-22)
501

2011.06 (Fol-22) - Method
501

2011.06 (Fol-22) - Results-Table 1
505

2011.06 (Fol-22) - Tables 2-3
507

2011.06 (Fol-22) - Figure 1/Table-4
510

2011.06 (Fol-22) - Figure 2/Table-5
511

2011.06 (Fol-22) - Table-6
512

2011.06 (Fol-22) - Figure 3-5
513

2011.06 (Fol-22) - Table 7-13
516

2011.06 (Fol-22) - Analysis of SPIFAN Matrices-Tables 14-17
520

2011.06 (Fol-22) - Folate Analysis-Table 18-22
527

2011.06 (Fol-22) - LOD/LOQ
533

2011.06 (Fol-22) - Conclusions
534

FRUCTANS (FOS)
537

Fructans (FOS) SMPR
537

Fos-01
539

Fos-01 - SLV
539

Fos-01 - Annex 1-Chromatogram
552

Fos-01 - Annex 2b-Calibration Curve-Sucrose
553

Fos-01 - Annex 3-Chromatogram (J4G0975 sample)
554

Fos-01 - Annex 4-Results for precision
555

Fos-01 - Annex 5-Results for the recovery
556

Fos-01 - MEF
557

Fos-04
563

Fos-04 - Method-Part 1
563

Fos-04 - Part 2
567

Fos-04 - Tables & Figures
568

Fos-04 - Appendix A (Figures/Chromatograms)
579

Fos-04 - Appendix B (Figures/Chromatograms)
591

Fos-04 - Appendix C (Table C-1)
601

Fos-04 - MEF
602

VITAMIN D
607

Vitamin D SMPR
607

VitD-17
609

VitD-17 - Method & Tables 1-7
609

VitD-17 - MEF
615

VitD-18
625

VitD-18 - Method
625

VitD-18 - Validation
635

VitD-18 - Tables 1-4/Figures 1-6
639

VitD-18 - Precision-Table 5
642

VitD-18 - LOQ/LOD-Table 6-7
644

VitD-18 - Recovery-Table 8-11
645

VitD-18 - Bias against SRM-Table 12
647

VitD-18 - Bias against Ref.Method-Table 13
648

VitD-18 - Chromatography
649

VitD-18 - References
651

VitD-18 - Appendices
652

VitD-18 - Appendix A
652

VitD-18 - Appendix B
654

VitD-18 - Appendix C
657

VitD-18 - Appendix D
658

VitD-18 - Appendix E
661

VitD-18 - Appendix F
662

VitD-18 - Appendix G
664

VitD-18 - MEF
665