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Parameter

Method Performance

Please

report in units as stated in SMPR!

Weighting

factor for

parameter

Suitability Ranking (1-

3-5)

(select from drop-down

list, 5 = best)

SPIFAN matrices

Applicable to all forms of infant, adult, and/or pediatric

formula (powders, ready-to-feed liquids, and liquid

concentrates).

Any combination of milk, soy, rice, whey, hydrolyzed

protein, starch, and amino acids, with and without intact

protein.

SLV Test Material Kit for FOS provided by

Covance

1

All analytes defined in the

applicability statement are

measured.

Fructans

g/100g reconstituted final product

1

0,03 - 5,0%

Analyte 1

not relevant

Analyte 2

Analyte 3

Analyte 4

Analyte 5

Analyte 1

0,03

0,03

Analyte 2

Analyte 3

Analyte 4

Analyte 5

Spike recovery (%)

90-110% of mean spiked recovery

100.3

2

Bias vs SRM

no SRM available

not applicable

3

6%

6

7

12%

b

Units

Limit of quantification (LOQ)

Method Reference #

AOAC 997.08

Method title:

Principle of the method:

Fructans in food products

enzymatic chromatographic method

SMPR Requirement

Analytical Range.

1

Notes:

Overall Score

Intermediate Reproducibility

(RSDiR)

Recommendation of ERP

2 years after First Action Status

Laboratory safety

Other Considerations

Evaluation of Method Performance vs. SMPR requirements.

Feedback from Users of the Method since being awarded

First Action

Official Methods

Status

Repeatability (RSDr)

Reproducibility (RSDR)

Accuracy/Recovery

ADDITIONAL EVALUATION PARAMETERS

AOAC SMPR: 2014.002

Limit of detection (LOD)

1

a

Concentrations apply to (1) "ready to feed liquids" "as-is"; (2) reconstituted powders (25 g into 200 g water); and (3) liquid concentrates diluted 1:1 by weight.

Did Method Author Consider ERP’s Method Specific

Recommendations

(See web link to specific method

comments):

Decision by ERP

Proprietary equipment

move to Final Action/repeal/remove/expand 2 year term

0

No unique proprietary equipment/accessories are required.

Method does not require any special safety precautions e.g. personal protection from highly toxic solvents.

3

1

2

Bias against established method

Analytical equipment

1

Adequate proof of performance via system suitability

Is there a bias Yes/No ?

Analytical equipment is commonly available in most labs.

SPIFAN ERP Checklist v 1.6

27.06.2013

Fos-01 (February 2016) - MEF

FOR ERP USE ONLY

DO NOT DISTRIBUTE