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Fonterra Co-operative Group

Page 28

Appendix F: Data—Bias Against Reference Method

Table 4: Results for bias experiment against reference method

Sample

Concentration (IU hg

-1

)

HPLC-UV

UPLC-MS/MS

Sample-1

9.1

9.0

Sample-2

9.9

10.7

Sample-3

7.7

8.2

Sample-4

8.2

8.4

Sample-5

10.2

10.8

Sample-6

10.3

11.1

Sample-7

6.9

4.8

Sample-8

12.6

9.7

Sample-9

7.0

5.6

Sample-10

5.9

8.9

Sample-11

8.9

4.2

Sample-12

8.7

9.1

Sample-13

7.7

8.1

Sample-14

4.4

4.4

Sample-15

9.9

10.9

Sample-16

13.7

15.5

Sample-17

13.8

15.2

Sample-18

15.1

16.2

Sample-19

14.7

16.1

Sample-20

14.9

15.9

Sample-21

10.3

10.9

Sample-22

15.8

15.2

Sample-23

9.5

10.5

Sample-24

9.8

10.5

Sample-25

9.8

10.3

Sample-26

10.1

10.7

Sample-27

9.9

10.2

Sample-28

10.0

11.0

Sample-29

22.5

24.1

Sample-30

9.3

9.6

Sample-31

10.0

11.1

Sample-32

10.5

10.6

Sample-33

10.2

10.5

Sample-34

8.0

8.6

Sample-35

12.3

12.5

VitD-18 (February 2016)

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