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7

Day 1

Day 2

Day 3

Day 4

Day 5

Day 6

Avg* RSD** Avg* RSD** Avg* RSD** Avg* RSD** Avg* RSD** Avg* RSD**

SRM 1849a

191

1.34

195

2.76

196

3.11

195

3.09

191

2.84

201

1.45

IF PHMB

230

1.36

235

0.17

234

0.63

228

0.87

231

0.71

237

1.13

IF PHSB

15.3 2.55 16.0 3.01 15.9 1.17 17.6 0.72

19.3

0.53 16.6 1.16

TF MB

492

0.39

514

0.21

526

1.18

494

0.96

496

0.15

509

0.47

IF MB

148

1.90

146

1.47

150

2.19

144

0.41

148

0.98

151

1.6

AN LF

55.7 3.37 59.7 4.83 55.0 4.01 58.1 0.64

52.6

5.01 58.6

4.1

CF

19.9 3.77 20.2 3.32 19.2 0.22 21.3 0.88

22.7

4.36 20.2 0.94

IE

Not found

IF FOS/GOS

681

0.92

666

0.44

671

2.10

670

0.26

635

0.79

686

4.26

IF MB(2)

214

3.40

219

0.03

205

0.06

231

2.94

199

2.63

236

2.81

IF SB

18.8 2.38 19.3 0.43 19.4 2.43 20.6 0.04

23.0

4.71 19.7 0.34

IF RTF MB

137

1.47

146

0.97

122

0.50

147

1.38

121

1.38

149

1.18

AN RTF HP

21.9 2.33 22.9 0.95 23.1 0.59 24.9 0.69

***

24.0 0.24

AN RTF HF

44.3 0.10 46.2 0.79 46.0 0.92 49.3 0.99

46.6

0.74 49.4 2.48

*

Conc.in

μg/100g

** RSD in %

*** Sample volume was not enough for injection (It is due to the human error and can be easily avoided)

Table 5. Fluoride 6 day validation data for intermediate precision, n = 2

Fluor-02/Chlor-03 (February 2016)

FOR ERP USE ONLY

DO NOT DISTRIBUTE