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Table 1

Accuracy - Spike Recovery

Avg (%)

RSD % Avg (%)

RSD (%)

Infant Formula Powder

vitamin D2

3

0.0

90.1

3.2

95.2

8.2

Infant Formula Powder

v

itamin D3

3

0.9 100.8

7.4

96.8

8.2

Milk Pwd DHA PREBIOTICS

vitamin D2

3

0.0

88.6

3.3

93.8

3.6

Milk Pwd DHA PREBIOTICS

v

itamin D3

3

1.0

98.5

4.8

98.3

7.6

DHA SOY

vitamin D2

3

0.0

92.9

3.0

93.2

0.9

DHA SOY

v

itamin D3

3

1.0 108.0

2.5 104.9

0.9

Adult Nutritional Ready To Feed (High Fat)

vitamin D2

3

0.0

97.3

3.9

91.0

2.0

Adult Nutritional Ready To Feed (High Fat)

v

itamin D3

3

1.2 102.3

4.8 101.8

2.4

Global Mean %

97.3

4.1

96.9

4.2

+ Spike Level 2

Spike Recovery

Product

Nr. replicates (n)

Native level

Analyte

Note:

The native level unit is μg/100g reconstituted milk powders. The spike level 1 of vitamin D2 is 0.05 μg/100g and the

level 2 is 0.1 μg/100g. The spike level 1 of vitamin D3 is 0.5μg/100g and the level 2 is 1.0μg/100g .

+ Spike Level 1

SPIFAN Code

SPIFAN ERP Checklist v1.0

VitD-17 MEF (February 2016)

FOR ERP USE ONLY

DO NOT DISTRIBUTE