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Choline 2012-20 MLT YKLP059 & ZNPI092.xls

Blind Duplicates of Powdered Samples -

YKLP059 & ZNPI092

Choline 2012-20 MLT YKLP059 & ZNPI092 -

Remove Labs 9-10-11.xls

Blind Duplicates of Powdered Samples –

YKLP059 & ZNPI092 with data from Labs 9, 10,

and 11 removed

Choline 2012-20 MLT LHTK069 & LKAU043.xls

Blind Duplicates of RTF Samples - LHTK069 &

LKAU043

Choline 2012-20 MLT MOPG098 & SJLQ035.xls Blind Duplicates of RTF Samples - MOPG098 &

SJLQ035

Choline 2012-20 MLT VFJL091 & YATV077.xls

Blind Duplicates of RTF Samples - VFJL091 &

YATV077

Final Results Table.docx

As titled

Here are a few quick observations on the results. Using the data from all eleven labs, with a

few labs that had results that were obviously far off the others, the blind duplicates data sheet

does not require the removal of any of the labs for the RTF samples. While for the powdered

samples, one lab’s data had to be removed for one of the blind duplicates, and same lab’s data

and the data from two additional labs had to be removed for another of the blind duplicates. In

general the study participants did better with the RTF samples, but this may be more related to

analyte concentrations because in the general the lower the sample’s choline concentration

was, the worse the results. Two labs purposely ran a different range of calibration standards.

These were the eleven participating labs.

Please note that the order listed below does not

correspond to the order in Table 2

, which has notes on each lab that are relevant to the study.

In Table 2 the first eight labs had the best data compared to the Single Lab Validation results.

I queried the participating labs if they had any comments on the method, and the comments I

received are in Appendix 2.

1.

Friesland-Campina - Netherlands

2.

GQT - China

3.

Thermo Fisher Scientific European Food Testing Lab - Germany

4.

Mead Johnson – US

5.

Mead Johnson – Singapore

6.

Mead Johnson - Netherlands

7.

Covance Laboratories - US

SUMMARY OF MLT

FOR ERP USE ONLY

DO NOT DISTRIBUTE