398-399 / 620
Table 1
Accuracy - Spike Recovery
Avg (%)
RSD % Avg (%)
RSD (%)
Child Formula Powder
00847RF00
Fluoride
9
70.1
82.4
4.51
81.5
2.45
Infant Elemental Powder
00796RF
Fluoride
IF milk based RTF
na
Fluoride
9
289
77.1
3.79
73.8
5.51
AN High-Protein RTF
00821RF00
Fluoride
9
809
110
7.42
166
14.8
AN High-Fat RTF
00820RF00
Fluoride
9
927
84.9
15.3
98.0
9.37
Global Mean % 88.6
7.8
104.8
8.0
Additional information to be completed by SD
yes
no
yes
yes
no
no
yes
yes
no
Analyte
Were all spike recovery samples prepared on multiple days?
Were spike recoveries calculated from theoretical additions?
Or was spiking solution analyzed and the results used to calculate spike recoveries?
+ Spike Level 1
SPIFAN Code
Was a portion of the product spiked?
Were all spike recovery samples taken from the same spiked product?
Were multiple portions of the product spiked and each spiked product analyzed?
Were products weighed into extraction vessels before spiking?
Were all spike recovery samples prepared on the same day?
Not found
+ Spike Level 2
Spike Recovery
a
Product
Nr. replicates (n)
Native level
Were products spiked before they were weighed into extraction vessels?
What form of the nutrient was spiked into the product?
What kind of solution or solvent was used to deliver the spike to the product?
What percentage of the spiked sample was the spiked was the spike blanc? (How much was product diluted by spike?)
a: Prepared over three
days, each preparation
injected three times
SPIFAN ERP Checklist v1.0
Fluor-02 - MEF FORM
FOR ERP USE ONLY
DO NOT DISTRIBUTE