SPIFAN Nutrients ERP Book 9-29-15

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Table 1 Accuracy - Spike Recovery
Avg (%) RSD % Avg (%) RSD (%)
Infant Powder Milk D04HTCVV Ca 3 days x triplicates 52.2 98.6 3.5
Infant Powder Soy E29JVLV Ca 3 days x triplicates 71.9 103 12.0
Infant Pwd Milk Part Hyd 1172572116 Ca 3 days x triplicates 46.6 98.4 8.6
Infant Pwd Soy Part Hyd 117257651Z Ca 3 days x triplicates 72.0 100 9.7
Adult Powder Low Fat 00394RF00 Ca 3 days x triplicates 30.5 99.6 8.0
Adult Pwd Milk 11750017V3 Ca 3 days x triplicates 31.3 101 4.2
Child Formula Pwd 00412RF00 Ca 3 days x triplicates 42.2 103 7.5
Infant Elemental Pwd 00403RF00 Ca 3 days x triplicates 70.1 101 12.5
Infant RTF Milk SPIFAN CTL Ca 3 days x triplicates 59.8 90.2 4.0
Adult RTF HP 00414RF00 Ca 3 days x triplicates 98.3 98.6 8.4
Adult RTF HF (falling apart) 00406RF00 Ca 3 days x triplicates 88.8 104 14.0
MEAN 99.6
Infant Powder Milk D04HTCVV Cu 3 days x triplicates 0.0603 90 2.1
Infant Powder Soy E29JVLV Cu 3 days x triplicates 0.0600 93.8 1.0
Infant Pwd Milk Part Hyd 1172572116 Cu 3 days x triplicates 0.0544 102 8.6
Infant Pwd Soy Part Hyd 117257651Z Cu 3 days x triplicates 0.0542 97.8 4.8
Adult Powder Low Fat 00394RF00 Cu 3 days x triplicates 0.0704 99.3 4.0
Adult Pwd Milk 11750017V3 Cu 3 days x triplicates 0.128 105 1.4
Child Formula Pwd 00412RF00 Cu 3 days x triplicates 0.0572 95.3 0.7
Infant Elemental Pwd 00403RF00 Cu 3 days x triplicates 0.0800 99.4 1.4
Infant RTF Milk SPIFAN CTL Cu 3 days x triplicates 0.0579 91.7 2.9
Adult RTF HP 00414RF00 Cu 3 days x triplicates 0.181 91.3 4.1
Adult RTF HF 00406RF00 Cu 3 days x triplicates 0.237 106 6.3
MEAN 97.4
Infant Powder Milk D04HTCVV Fe 3 days x triplicates 1.29 98.4 4.6
Infant Powder Soy E29JVLV Fe 3 days x triplicates 1.26 96.9 4.6
Infant Pwd Milk Part Hyd 1172572116 Fe 3 days x triplicates 0.930 97.1 6.3
Infant Pwd Soy Part Hyd 117257651Z Fe 3 days x triplicates 1.23 96.8 6.5
Adult Powder Low Fat 00394RF00 Fe 3 days x triplicates 0.664 98.8 7.4
Adult Pwd Milk 11750017V3 Fe 3 days x triplicates 0.487 98.3 3.7
Child Formula Pwd 00412RF00 Fe 3 days x triplicates 0.641 101 2.2
Infant Elemental Pwd 00403RF00 Fe 3 days x triplicates 1.16 99.8 5.2
Infant RTF Milk SPIFAN CTL Fe 3 days x triplicates 1.43 92.8 3.8
Adult RTF HP 00414RF00 Fe 3 days x triplicates 1.87 97.3 8.1
Adult RTF HF 00406RF00 Fe 3 days x triplicates 2.15 99.3 9.1
MEAN 97.9
Infant Powder Milk D04HTCVV Mg 3 days x triplicates 6.28 101 9.0
Infant Powder Soy E29JVLV Mg 3 days x triplicates 8.07 103 8.8
Infant Pwd Milk Part Hyd 1172572116 Mg 3 days x triplicates 4.19 104 5.2
Infant Pwd Soy Part Hyd 117257651Z Mg 3 days x triplicates 6.72 103 11.3
Adult Powder Low Fat 00394RF00 Mg 3 days x triplicates 12.55 102 8.3
Adult Pwd Milk 11750017V3 Mg 3 days x triplicates 4.78 104 4.0
Child Formula Pwd 00412RF00 Mg 3 days x triplicates 8.24 104 9.8
Infant Elemental Pwd 00403RF00 Mg 3 days x triplicates 5.43 100 4.5
Infant RTF Milk SPIFAN CTL Mg 3 days x triplicates 5.94 93.0 2.7
Adult RTF HP 00414RF00 Mg 3 days x triplicates 33.0 92.8 9.9
Adult RTF HF 00406RF00 Mg 3 days x triplicates 39.8 99.2 9.0
3 days x triplicates MEAN 100.5
Infant Powder Milk D04HTCVV Mn 3 days x triplicates 0.0117 99.6 5.5
Infant Powder Soy E29JVLV Mn 3 days x triplicates 0.0368 94.9 3.5
Infant Pwd Milk Part Hyd 1172572116 Mn 3 days x triplicates 0.0117 98.9 7.0
Infant Pwd Soy Part Hyd 117257651Z Mn 3 days x triplicates 0.0256 101 0.6
Adult Powder Low Fat 00394RF00 Mn 3 days x triplicates 0.1555 101 4.8
Adult Pwd Milk 11750017V3 Mn 3 days x triplicates 0.0589 99.5 5.6
Child Formula Pwd 00412RF00 Mn 3 days x triplicates 0.0847 95.3 0.7
Infant Elemental Pwd 00403RF00 Mn 3 days x triplicates 0.0519 99.6 5.6
Infant RTF Milk SPIFAN CTL Mn 3 days x triplicates 0.0153 93.5 2.2
Adult RTF HP 00414RF00 Mn 3 days x triplicates 0.422 94.3 4.4
Adult RTF HF 00406RF00 Mn 3 days x triplicates 0.480 99.7 8.0
3 days x triplicates MEAN 97.9
Infant Powder Milk D04HTCVV P 3 days x triplicates 31.1 102 6.8
Infant Powder Soy E29JVLV P 3 days x triplicates 47.2 108 5.3
Infant Pwd Milk Part Hyd 1172572116 P 3 days x triplicates 25.6 102 6.8
Infant Pwd Soy Part Hyd 117257651Z P 3 days x triplicates 43.9 100 2.7
Adult Powder Low Fat 00394RF00 P 3 days x triplicates 30.1 98.1 6.8
Adult Pwd Milk 11750017V3 P 3 days x triplicates 23.7 100 2.9
Child Formula Pwd 00412RF00 P 3 days x triplicates 38.8 106 3.2
Infant Elemental Pwd 00403RF00 P 3 days x triplicates 50.7 107 1.3
Infant RTF Milk SPIFAN CTL P 3 days x triplicates 29.8 99.9 2.9
Adult RTF HP 00414RF00 P 3 days x triplicates 95.1 100 2.9
Adult RTF HF 00406RF00 P 3 days x triplicates 101 109 2.8
3 days x triplicates MEAN 102.9
Infant Powder Milk D04HTCVV K 3 days x triplicates 75.0 104 16.0
Infant Powder Soy E29JVLV K 3 days x triplicates 83.8 110 12.0
Infant Pwd Milk Part Hyd 1172572116 K 3 days x triplicates 71.7 101 7.1
Infant Pwd Soy Part Hyd 117257651Z K 3 days x triplicates 82.2 98.0 6.6
Adult Powder Low Fat 00394RF00 K 3 days x triplicates 56.3 108 5.3
Adult Pwd Milk 11750017V3 K 3 days x triplicates 64.5 103 1.3
Child Formula Pwd 00412RF00 K 3 days x triplicates 61.1 105 10.6
Infant Elemental Pwd 00403RF00 K 3 days x triplicates 88.6 99.2 10.0
Infant RTF Milk SPIFAN CTL K 3 days x triplicates 100 108 13.0
Adult RTF HP 00414RF00 K 3 days x triplicates 156 92.4 11.0
Adult RTF HF 00406RF00 K 3 days x triplicates 236 105 8.2
3 days x triplicates MEAN 103.0
Infant Powder Milk D04HTCVV Na 3 days x triplicates 20.8 102 4.5
Infant Powder Soy E29JVLV Na 3 days x triplicates 25.6 106 7.6
Infant Pwd Milk Part Hyd 1172572116 Na 3 days x triplicates 17.4 101 2.3
Infant Pwd Soy Part Hyd 117257651Z Na 3 days x triplicates 27.4 99.8 3.6
Adult Powder Low Fat 00394RF00 Na 3 days x triplicates 23.0 103 5.5
Adult Pwd Milk 11750017V3 Na 3 days x triplicates 25.2 105 2.7
Child Formula Pwd 00412RF00 Na 3 days x triplicates 16.2 106 6.8
Infant Elemental Pwd 00403RF00 Na 3 days x triplicates 26.8 106 11.0
Spike Recovery
Product Nr. replicates (n) Native level
mg/100g as RTF
Analyte 50-200% Native SPIFAN Code
SPIFAN ERP Checklist v1.0
MTE-02 MEF Form
FOR ERP USE ONLY
DO NOT DISTRIBUTE