SPIFAN Nutrients ERP Book 9-29-15

452 / 620

Table 3
Product SPIFAN Code Analyte2 Nr. replicates (n) 3 Conc. Level mg/100g
RTF RSDr1 RSD iR
Conc. Level
mg/100g RSDr RSD iR
Infant Powder Milk D04HTCVV Ca 8 days x 2 reps 52.2 <5% 2.5 X ≤ Z % ≤ W %
Infant Powder Soy E29JVLV Ca 8 days x 2 reps 71.9 <5% 3.5 Ca,Cu,Fe,Mg,P,K,Na,Zn entire range 5.0% none
Infant Pwd Milk Part Hyd 1172572116 Ca 8 days x 2 reps 46.6 <5% 2.2 Mn 0.001-0.005 8.0% none
Infant Pwd Soy Part Hyd 117257651Z Ca 8 days x 2 reps 72.0 <5% 2.2 Mn 0.005-1.0 5.0% none
Adult Powder Low Fat 00394RF00 Ca 8 days x 2 reps 30.5 <5% 2.7
Adult Pwd Milk 11750017V3 Ca 8 days x 2 reps 31.3 <5% 2.3
Child Formula Pwd 00412RF00 Ca 8 days x 2 reps 42.2 <5% 1.8
Infant Elemental Pwd 00403RF00 Ca 8 days x 2 reps 70.1 <5% 2.2
Infant RTF Milk SPIFAN CTL Ca 8 days x 2 reps 59.8 <5% 4.5
Adult RTF HP 00414RF00 Ca 8 days x 2 reps 98.3 <5% 2.8
Adult RTF HF (product has fallen apart) 00406RF00 Ca 8 days x 2 reps 88.8 <5% 9.4!
Global Mean % <5% 2.7
Infant Powder Milk D04HTCVV Cu 8 days x 2 reps 0.0603 <5% 4.9 Ca,Cu,Fe,Mg,P,K,Na,Zn entire range 5.0% none
Infant Powder Soy E29JVLV Cu 8 days x 2 reps 0.0600 <5% 4.1 Mn 0.001-0.005 8.0% none
Infant Pwd Milk Part Hyd 1172572116 Cu 8 days x 2 reps 0.0544 <5% 3.9 Mn 0.005-1.0 5.0% none
Infant Pwd Soy Part Hyd 117257651Z Cu 8 days x 2 reps 0.0542 <5% 3.9
Adult Powder Low Fat 00394RF00 Cu 8 days x 2 reps 0.0704 <5% 3.3
Adult Pwd Milk 11750017V3 Cu 8 days x 2 reps 0.128 <5% 3.3
Child Formula Pwd 00412RF00 Cu 8 days x 2 reps 0.0572 <5% 3.7
Infant Elemental Pwd 00403RF00 Cu 8 days x 2 reps 0.0800 <5% 1.7
Infant RTF Milk SPIFAN CTL Cu 8 days x 2 reps 0.0579 <5% 3.5
Adult RTF HP 00414RF00 Cu 8 days x 2 reps 0.181 <5% 3.0
Adult RTF HF 00406RF00 Cu 8 days x 2 reps 0.237 <5% 3.0
Global Mean % <5% 3.5
Infant Powder Milk D04HTCVV Fe 8 days x 2 reps 1.29 <5% 2.0 Ca,Cu,Fe,Mg,P,K,Na,Zn entire range 5.0% none
Infant Powder Soy E29JVLV Fe 8 days x 2 reps 1.26 <5% 2.4 Mn 0.001-0.005 8.0% none
Infant Pwd Milk Part Hyd 1172572116 Fe 8 days x 2 reps 0.930 <5% 3.1 Mn 0.005-1.0 5.0% none
Infant Pwd Soy Part Hyd 117257651Z Fe 8 days x 2 reps 1.23 <5% 2.5
Adult Powder Low Fat 00394RF00 Fe 8 days x 2 reps 0.664 <5% 3.5
Adult Pwd Milk 11750017V3 Fe 8 days x 2 reps 0.487 <5% 4.0
Child Formula Pwd 00412RF00 Fe 8 days x 2 reps 0.641 <5% 3.2
Infant Elemental Pwd 00403RF00 Fe 8 days x 2 reps 1.16 <5% 1.9
Infant RTF Milk SPIFAN CTL Fe 8 days x 2 reps 1.43 <5% 4.3
Adult RTF HP 00414RF00 Fe 8 days x 2 reps 1.87 <5% 3.4
Adult RTF HF 00406RF00 Fe 8 days x 2 reps 2.15 <5% 3.6
Global Mean % <5% 3.1
Infant Powder Milk D04HTCVV Mg 8 days x 2 reps 6.28 <5% 2.9 Ca,Cu,Fe,Mg,P,K,Na,Zn entire range 5.0% none
Infant Powder Soy E29JVLV Mg 8 days x 2 reps 8.07 <5% 2.8 Mn 0.001-0.005 8.0% none
Infant Pwd Milk Part Hyd 1172572116 Mg 8 days x 2 reps 4.19 <5% 2.6 Mn 0.005-1.0 5.0% none
Infant Pwd Soy Part Hyd 117257651Z Mg 8 days x 2 reps 6.72 <5% 2.9
Adult Powder Low Fat 00394RF00 Mg 8 days x 2 reps 12.55 <5% 2.9
Adult Pwd Milk 11750017V3 Mg 8 days x 2 reps 4.78 <5% 3.3
Child Formula Pwd 00412RF00 Mg 8 days x 2 reps 8.24 <5% 2.5
Infant Elemental Pwd 00403RF00 Mg 8 days x 2 reps 5.43 <5% 3.3
Infant RTF Milk SPIFAN CTL Mg 8 days x 2 reps 5.94 <5% 3.1
Adult RTF HP 00414RF00 Mg 8 days x 2 reps 33.0 <5% 3.4
Adult RTF HF 00406RF00 Mg 8 days x 2 reps 39.8 <5% 1.8
Global Mean % <5% 2.9
Infant Powder Milk D04HTCVV Mn 8 days x 2 reps 0.0117 <5% 2.0 Ca,Cu,Fe,Mg,P,K,Na,Zn entire range 5.0% none
Infant Powder Soy E29JVLV Mn 8 days x 2 reps 0.0368 <5% 2.3 Mn 0.001-0.005 8.0% none
Infant Pwd Milk Part Hyd 1172572116 Mn 8 days x 2 reps 0.0117 <5% 2.6 Mn 0.005-1.0 5.0% none
Infant Pwd Soy Part Hyd 117257651Z Mn 8 days x 2 reps 0.0256 <5% 2.6
Adult Powder Low Fat 00394RF00 Mn 8 days x 2 reps 0.1555 <5% 2.7
Adult Pwd Milk 11750017V3 Mn 8 days x 2 reps 0.0589 <5% 2.6
Child Formula Pwd 00412RF00 Mn 8 days x 2 reps 0.0847 <5% 1.4
Infant Elemental Pwd 00403RF00 Mn 8 days x 2 reps 0.0519 <5% 1.3
Infant RTF Milk SPIFAN CTL Mn 8 days x 2 reps 0.0153 <5% 2.9
Adult RTF HP 00414RF00 Mn 8 days x 2 reps 0.422 <5% 2.1
Adult RTF HF 00406RF00 Mn 8 days x 2 reps 0.480 <5% 4.8
Global Mean % <5% 2.5
Infant Powder Milk D04HTCVV P 8 days x 2 reps 31.1 <5% 1.7 Ca,Cu,Fe,Mg,P,K,Na,Zn entire range 5.0% none
Infant Powder Soy E29JVLV P 8 days x 2 reps 47.2 <5% 5.0 Mn 0.001-0.005 8.0% none
Infant Pwd Milk Part Hyd 1172572116 P 8 days x 2 reps 25.6 <5% 4.4 Mn 0.005-1.0 5.0% none
Infant Pwd Soy Part Hyd 117257651Z P 8 days x 2 reps 43.9 <5% 3.6
Adult Powder Low Fat 00394RF00 P 8 days x 2 reps 30.1 <5% 1.8
Adult Pwd Milk 11750017V3 P 8 days x 2 reps 23.7 <5% 2.4
Child Formula Pwd 00412RF00 P 8 days x 2 reps 38.8 <5% 2.0
Infant Elemental Pwd 00403RF00 P 8 days x 2 reps 50.7 <5% 2.4
Infant RTF Milk SPIFAN CTL P 8 days x 2 reps 29.8 <5% 4.3
Adult RTF HP 00414RF00 P 8 days x 2 reps 95.1 <5% 3.4
Adult RTF HF 00406RF00 P 8 days x 2 reps 101 <5% 2.9
Global Mean % <5% 3.1
Infant Powder Milk D04HTCVV K 8 days x 2 reps 75.0 <5% 3.3 Ca,Cu,Fe,Mg,P,K,Na,Zn entire range 5.0% none
Infant Powder Soy E29JVLV K 8 days x 2 reps 83.8 <5% 2.6 Mn 0.001-0.005 8.0% none
Infant Pwd Milk Part Hyd 1172572116 K 8 days x 2 reps 71.7 <5% 1.1 Mn 0.005-1.0 5.0% none
Infant Pwd Soy Part Hyd 117257651Z K 8 days x 2 reps 82.2 <5% 2.2
Adult Powder Low Fat 00394RF00 K 8 days x 2 reps 56.3 <5% 2.1
Adult Pwd Milk 11750017V3 K 8 days x 2 reps 64.5 <5% 1.7
Child Formula Pwd 00412RF00 K 8 days x 2 reps 61.1 <5% 2.5
Infant Elemental Pwd 00403RF00 K 8 days x 2 reps 88.6 <5% 3.1
Infant RTF Milk SPIFAN CTL K 8 days x 2 reps 100 <5% 3.0
Adult RTF HP 00414RF00 K 8 days x 2 reps 156 <5% 3.9
Adult RTF HF 00406RF00 K 8 days x 2 reps 236 <5% 1.7
Global Mean % <5% 2.5
Infant Powder Milk D04HTCVV Na 8 days x 2 reps 20.8 <5% 3.2 Ca,Cu,Fe,Mg,P,K,Na,Zn entire range 5.0% none
Infant Powder Soy E29JVLV Na 8 days x 2 reps 25.6 <5% 2.4 Mn 0.001-0.005 8.0% none
Infant Pwd Milk Part Hyd 1172572116 Na 8 days x 2 reps 17.4 <5% 1.8 Mn 0.005-1.0 5.0% none
Infant Pwd Soy Part Hyd 117257651Z Na 8 days x 2 reps 27.4 <5% 2.9
Adult Powder Low Fat 00394RF00 Na 8 days x 2 reps 23.0 <5% 2.8
Adult Pwd Milk 11750017V3 Na 8 days x 2 reps 25.2 <5% 2.2
Child Formula Pwd 00412RF00 Na 8 days x 2 reps 16.2 <5% 2.6
Infant Elemental Pwd 00403RF00 Na 8 days x 2 reps 26.8 <5% 3.0
Infant RTF Milk SPIFAN CTL Na 8 days x 2 reps 17.8 <5% 2.2
Adult RTF HP 00414RF00 Na 8 days x 2 reps 102 <5% 1.9
Adult RTF HF 00406RF00 Na 8 days x 2 reps 139 <5% 2.0
Global Mean % <5% 2.5
Infant Powder Milk D04HTCVV Zn 8 days x 2 reps 0.732 <5% 1.5 Ca,Cu,Fe,Mg,P,K,Na,Zn entire range 5.0% none
Infant Powder Soy E29JVLV Zn 8 days x 2 reps 0.821 <5% 2.3 Mn 0.001-0.005 8.0% none
Infant Pwd Milk Part Hyd 1172572116 Zn 8 days x 2 reps 0.482 <5% 2.6 Mn 0.005-1.0 5.0% none
Infant Pwd Soy Part Hyd 117257651Z Zn 8 days x 2 reps 0.547 <5% 1.8
Adult Powder Low Fat 00394RF00 Zn 8 days x 2 reps 0.690 <5% 2.6
Adult Pwd Milk 11750017V3 Zn 8 days x 2 reps 0.582 <5% 2.6
Child Formula Pwd 00412RF00 Zn 8 days x 2 reps 0.418 <5% 1.7
Infant Elemental Pwd 00403RF00 Zn 8 days x 2 reps 0.718 <5% 2.1
Infant RTF Milk SPIFAN CTL Zn 8 days x 2 reps 0.717 <5% 2.1
Adult RTF HP 00414RF00 Zn 8 days x 2 reps 2.20 <5% 2.4
Adult RTF HF 00406RF00 Zn 8 days x 2 reps 2.79 <5% 1.4
Global Mean % <5% 2.1
Infant Powder Milk D04HTCVV Cr 8 days x 2 reps 4.9 <5% 7.7 (<QL) Cr 20-1600 µg/kg 5.0% none
Infant Powder Soy E29JVLV Cr 8 days x 2 reps 8.1 <5% 5.2 (<QL) Mo 20-1000 µg/kg 5.0% none
Infant Pwd Milk Part Hyd 1172572116 Cr 8 days x 2 reps 2.4 <5% 20 (<QL) Se 10-200 µg/kg 5.0% none
Infant Pwd Soy Part Hyd 117257651Z Cr 8 days x 2 reps 6.0 <5% 9.2 (<QL)
Adult Powder Low Fat 00394RF00 Cr 8 days x 2 reps 47.6 <5% 1.3
Adult Pwd Milk 11750017V3 Cr 8 days x 2 reps 15.8 <5% 5.0 (<QL)
Child Formula Pwd 00412RF00 Cr 8 days x 2 reps 30.2 <5% 1.3
Infant Elemental Pwd 00403RF00 Cr 8 days x 2 reps 23.9 <5% 6.3
Infant RTF Milk SPIFAN CTL Cr 8 days x 2 reps 7.6 <5% 53 (<QL)
Adult RTF HP 00414RF00 Cr 8 days x 2 reps 130 <5% 2.9
Adult RTF HF 00406RF00 Cr 8 days x 2 reps 141 <5% 1.8
Global Mean % <5% 2.7
Infant Powder Milk D04HTCVV Mo 8 days x 2 reps 17.7 <5% 8.2 (<QL) Cr 20-1600 µg/kg 5.0% none
Infant Powder Soy E29JVLV Mo 8 days x 2 reps 36.5 <5% 4.5 Mo 20-1000 µg/kg 5.0% none
Infant Pwd Milk Part Hyd 1172572116 Mo 8 days x 2 reps 20.4 <5% 4.0 Se 10-200 µg/kg 5.0% none
Infant Pwd Soy Part Hyd 117257651Z Mo 8 days x 2 reps 33.0 <5% 3.6
Adult Powder Low Fat 00394RF00 Mo 8 days x 2 reps 62.7 <5% 3.0
Adult Pwd Milk 11750017V3 Mo 8 days x 2 reps 32.6 <5% 4.9
Child Formula Pwd 00412RF00 Mo 8 days x 2 reps 30.0 <5% 5.1
Infant Elemental Pwd 00403RF00 Mo 8 days x 2 reps 17.8 <5% 7.5 (<QL)
Infant RTF Milk SPIFAN CTL Mo 8 days x 2 reps 16.9 <5% 10 (<QL)
Adult RTF HP 00414RF00 Mo 8 days x 2 reps 154 <5% 3.2
Adult RTF HF 00406RF00 Mo 8 days x 2 reps 193 <5% 2.6
Global Mean % <5% 3.9
Infant Powder Milk D04HTCVV Se 8 days x 2 reps 25.6 <5% 6.5 Cr 20-1600 µg/kg 5.0% none
Infant Powder Soy E29JVLV Se 8 days x 2 reps 24.8 <5% 3.3 Mo 20-1000 µg/kg 5.0% none
Infant Pwd Milk Part Hyd 1172572116 Se 8 days x 2 reps 26.6 <5% 2.7 Se 10-200 µg/kg 5.0% none
Infant Pwd Soy Part Hyd 117257651Z Se 8 days x 2 reps 26.8 <5% 4.1
Adult Powder Low Fat 00394RF00 Se 8 days x 2 reps 29.7 <5% 3.2
Adult Pwd Milk 11750017V3 Se 8 days x 2 reps 24.3 <5% 2.8
Child Formula Pwd 00412RF00 Se 8 days x 2 reps 23.7 <5% 2.9
Infant Elemental Pwd 00403RF00 Se 8 days x 2 reps 23.2 <5% 2.8
Infant RTF Milk SPIFAN CTL Se 8 days x 2 reps 29.6 <5% 2.9
Adult RTF HP 00414RF00 Se 8 days x 2 reps 92.6 <5% 3.0
Adult RTF HF 00406RF00 Se 8 days x 2 reps 133 <5% 3.6
Global Mean % <5% 3.4
1 Method requires duplicates to be run, and the RSD to be <5% for them; thus, adequate repeatability is built into the method (typically RSD is 1-2%)
2 all analytes ratioed to Ge internal standard except for Se, which uses Te
3 4 days on an Agilent 7500, 4 days on an Agilent 7700, rotating 2 analysts throughout
powders changed to RTF basis (divided by 9)
Precision - repeatability.
REQUIREMENTS SMPR
SPIFAN ERP X Checklist v 1.0
MTE-02 MEF Form
FOR ERP USE ONLY
DO NOT DISTRIBUTE