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© 2015 AOAC INTERNATIONAL
(
d
)
Standard Method Performance Requirements
(AOAC
SMPR® 2012.007; 1) for repeatability, reproducibility, and
recovery for the method are shown in the Table
2015.01J
.
See
AppendixA (available on the
J. AOAC Int
. website as supplemental
material,
http://aoac.publisher.ingentaconnect.com/content/aoac/jaoac) for detailed method performance information supporting
acceptance of the method.
(
e
)
See
AppendixAfor detailedmethod performance information
supporting acceptance of the method. Method validation samples
were prepared and analyzed for all applicable matrices. In general,
all SMPR criteria were met for As, Cd, Hg, and Pb in the matrices
apple juice, infant formula, cocoa powder, and rice flour.
References: (1) AOAC SMPR 2012.007
J. AOAC Int . 96 , 704(2013)DOI: 10.5740/jaoac.int.2012.007
J. AOAC Int . 98 , 1113(2015)DOI: 10.5740/jaoac.int.2015.01
Posted: September 9, 2015
Table 2015.01J. AOAC SMPR 2012.007 (ref. 1)
Concn range, μg/kg Repeatability, % Reproducibility, % Recovery, %
LOQ–100
15
32
60–115
100–1000
11
16
80–115
>1000
7.3
8
80–115
Candidates for 2016 Method of the Year
11