44 / 112
110
H
ALBMAYR
-J
ECH
ET AL
.
:
J
OURNAL OF
AOAC I
NTERNATIONAL
V
OL
. 98, N
O
. 1, 2015
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be used
Sample ID
a
Lab
Sample 1
Sample 2
Sample 3
Sample 4
Sample 5
Sample 6
Sample 7
Sample 8
Sample 9
Sample 10
Sample 11
Sample 12
A 0, 7 0, 3 14, 1 18, 3 21, 4 23, 1 107, 5 115, 5 –1, 1 0, 1 4, 6 4, 7 12, 4 10, 1 61, 0 59, 5 2, 5 3, 2 12, 0 13, 7 26, 5 24, 9 92, 1 109, 9
D 1, 1 3, 6 18, 5 17, 6 39, 8 53, 9 150, 5 162, 8 0, 9 0, 3 9, 3 7, 1 16, 2 17, 3 121.4
b
120.7
b
5, 8 3, 7 16, 8 18, 2 45, 0 41, 6 154, 5 159, 7
E 0, 4 0, 6 17, 7 14, 7 19, 1 48, 6 149, 1 177, 6 0, 9 –1, 2 6, 7 6, 1 12, 6 15, 9 79, 7 78, 5 0, 3 0, 5 11, 8 11, 0 17, 8 19, 9 102, 0 104, 9
F
0, 2 0, 4 11, 4 15, 6 19, 2 10, 2 58, 1 71, 2 0, 0 –2, 1 5, 3 5, 4 12, 1 10, 9 71, 2 62, 3 6, 7 2, 0 12, 0 9, 1 18, 8 18, 4 86, 7 79, 3
G 1, 2 0, 8 9, 1 14, 6 27, 3 26, 3 76, 7 70, 4 0, 5 –0, 9 7, 2 4, 9 12, 0 11, 6 52, 2 55, 4 4, 0 3, 0 13, 5 13, 8 22, 2 27, 0 103, 6 86, 5
H –0, 2 –0, 3 7, 7 7, 2 12, 6 14, 1 64, 2 60, 8 0, 7 0, 3 5, 3 6, 1 11, 9 13, 1 60, 4 59, 9 0, 7 0, 6 9, 1 8, 9 17, 3 16, 4 73, 8 66, 3
I
2, 0 2, 8 15, 6 12, 9 22, 7 19, 0 81, 5 78, 0 –1, 3 1, 9 3, 9 7, 1 10, 1 11, 7 51, 1 39, 0 5, 5 4, 9 15, 2 15, 0 39, 3 26, 2 65, 8 100, 4
K 6, 7 5, 6 15, 7 15, 5 38, 7 29, 9 85, 6 76, 0 0, 4 –0, 8 4, 3 4, 5 8, 9 11, 2 40, 1 39, 4 13.5
b
14.6
b
26, 0 23, 3 36, 4 36, 8 158, 4 114, 6
L
8.9
c
0.5
c
22, 0 17, 5 38, 3 56, 8 120, 5 143, 2 2, 9 –1, 7 9, 8 9, 1 12, 9 15, 1 66, 2 75, 4 3, 0 4, 7 13, 4 17, 2 34, 9 21, 4 118, 5 175, 7
M 3, 9 3, 5 18, 5 17, 7 20, 3 38, 9 99, 6 81, 4 0, 6 –0, 4 5, 3 7, 6 15, 5 13, 6 70, 3 78, 8 6, 9 11, 1 21, 3 19, 7 16, 9 21, 1 154, 6 90, 3
N 1, 7 4, 7 9, 7 12, 7 18, 9 15, 0 145, 0 111, 6 0, 1 0, 9 4, 5 3,8 9,6 9,5 45,5 52,0 4,8 10,9 11,1 10,4 20,6 23,8 102,1 90,5
O 1,3 1,9 15, 9 7, 4 26, 2 36, 2 124, 5 95, 6 0.3
c
1.5
c
6, 8 4, 9 18, 7 13, 9 73.6
c
108.7
c
4, 4 1, 6 19, 3 15, 3 26, 7 27, 5 144, 8 142, 8
P –0, 6 1, 1 7, 7 11, 1 14, 5 14, 2 74, 1 74, 5 0, 5 0, 1 7, 5 7, 0 13, 7 12, 7 71, 3 66, 1 6, 6 3, 5 12, 0 16, 4 22, 9 18, 7 75, 7 70, 8
Q 0, 3 0, 6 12, 6 10, 3 18, 9 13, 7 114, 9 108, 1 –0, 7 –1, 2 5, 3 6, 6 12, 1 13, 2 67, 7 69, 7 2, 5 2, 3 12, 6 11, 3 23, 2 20, 3 112, 9 99, 8
R 3, 3 3, 6 11, 3 15, 2 25, 2 32, 2 139, 4 93, 1 0, 3 0, 1 6, 5 6, 4 14, 1 12, 8 72, 6 70, 5 6, 4 6, 6 19, 3 19, 1 46, 0 38, 9 178, 5 152, 9
S 0, 8 1, 0 9, 9 7, 6 31, 9 17, 9 92, 3 58, 7 0, 9 0, 3 5, 7 3, 8 10, 8 10, 3 44, 1 55, 1 1, 3 2, 0 12, 4 11, 9 28, 6 18, 2 109, 2 60, 7
T –1, 1 –1, 4 10, 1 9, 3 21, 0 22, 7 95, 2 77, 8 0, 2 0, 1 6, 6 4, 6 14, 2 14, 2 71, 8 76, 9 1, 7 1, 1 9, 8 10, 6 19, 8 20, 0 109, 7 129, 0
U 2, 5 2, 8 16, 4 17, 7 26, 5 29, 0 97, 0 109, 4 –2.28
b
–2.74
b
11, 0 7, 8 17, 3 17, 9 76, 9 91, 2 4, 6 8, 4 19, 6 22, 7 33, 4 41, 4 139, 6 141, 3
a
*OXWHQ IUHH ULFH ÀRXU ULFH ÀRXU
PJ JOXWHQ NJ ULFH ÀRXU
PJ JOXWHQ NJ ULFH ÀRXU
PJ JOXWHQ NJ JOXWHQ IUHH FKRFRODWH FDNH FKRFRODWH FDNH PJ JOXWHQ NJ FKRFRODWH FDNH PJ
gluten/kg; 8 = chocolate cake 100 mg gluten/kg; 9 = crisp bread 4.5 mg gluten/kg; 10 = crisp bread 15 mg gluten/kg; 11 = crisp bread 24 mg gluten/kg; and 12 = crisp bread 102 mg gluten/kg.
b
Grubbs outlier.
c
Cochran outlier.