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SRM 3277

Krill Oil

Coordinated measurement of fatty acids and astaxanthin through Grocery Manufacturer’s

Association.

SRM 3278

Tocopherols in Edible Oils (TPL/TC)

Certification range extended based on stability data.

SRM 3281

Cranberry (Fruit)

Measured organic acids by ID-LC-MS and ID-GC-MS. Method developed for measurement of

anthocyanidins and flavonols by LC-Abs. Method developed for measurement of anthocyanins

by LC-Abs. Method developed for fingerprinting of proanthocyanidins by LC-FL-MS.

Conducted stability testing of organic acids by LC-MS.

SRM 3282

Low-Calorie Cranberry Juice Cocktail

Measured organic acids by IC-CD and LC-UV, method developed for measurement of

anthocyanidins and flavonols by LC-Abs. Conducted stability testing of organic acids by LC-

MS.

SRM 3283

Cranberry Extract

Measured organic acids by IC-CD and ID-LC-MS, method developed for measurement of

anthocyanidins and flavonols by LC-Abs. Method developed for measurement of anthocyanins

by LC-Abs. Method developed for fingerprinting of proanthocyanidins by LC-FL-MS.

Conducted stability testing of organic acids by LC-MS.

SRM 3284

Cranberry-Containing Solid Oral Dosage Form

Measured organic acids by IC-CD and ID-LC-MS, method developed for measurement of

anthocyanidins and flavonols by LC-Abs. Method developed for measurement of anthocyanins

by LC-Abs. Method developed for fingerprinting of proanthocyanidins by LC-FL-MS.

Conducted stability testing of organic acids by LC-MS.

SRM 3285

Mixed Berry-Containing Solid Oral Dosage Form

Measured organic acids by IC-CD and ID-LC-MS, method developed for measurement of

anthocyanidins and flavonols by LC-Abs. Method developed for measurement of anthocyanins

by LC-Abs. Method developed for fingerprinting of proanthocyanidins by LC-FL-MS.

Conducted stability testing of organic acids by LC-MS.

SRM 3286

Organic Acids Calibration Solution (TPL/TC)

Prepared and measured organic acids by LC-UV. Drafted and finalized Certificate of Analysis.

Conducted stability testing of organic acids by LC-MS.

SRM 3287

Blueberry (Fruit)

Measured organic acids by IC-CD and ID-LC-MS, method developed for measurement of

anthocyanidins and flavonols by LC-Abs. Method developed for measurement of anthocyanins

by LC-Abs. Method developed for fingerprinting of proanthocyanidins by LC-FL-MS.

Measured water-soluble vitamins by ID-LC-MS. Conducted stability testing of organic acids by

LC-MS.

SRM 3290

Dry Cat Food (TPL/TC)

Measured water-soluble vitamins by ID-LC/MS/MS. Measured choline and carnitine by ID-LC-

MS (via Grace Hahm, student intern). Coordinated measurement of total nutrients, gravimetric

fat, and crude fiber through Grocery Manufacturer’s Association. Collected final data and

prepared Report of Analysis summary for total nutrients. Prepared data for submission to SED.

Drafted and finalized Certificate of Analysis.

SRM 3291

Bilberry Extract

Measured organic acids by ID-LC-MS, method developed for measurement of organic acids by

AOAC OMB Meeting Book

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