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Pharmacology and Toxicology Research Laboratories, Inc., Clays Ferry, KY

Analytical Chemist II

1986 –1989

Provided chemical and biological analyses of drugs and their metabolites in serum;

developed and validated chemical analyses of pesticides and their metabolites in air, water,

soil, plant, and animal tissues in accordance to FDA and EPA guidelines. Other

responsibilities included experimental method development and in-house validation

certifications. Administrative Responsibilities included enforcement of in-house

regulations for radiological safety and decontamination of biohazards and/or radioactive

materials.

Primary chemist responsible for all analytical instruments, including Agilent 5890 GC with

ECD and NPD detectors, Agilent 5890 GC-MSD, HP 1010 HPLC with UV/Visible and

Fluorescence detectors, and various scintillation counters.

University of Kentucky, College of Agriculture, Lexington, KY

Principal Laboratory Technician, Agronomy Department

1985 –1986

Analytical responsibilities for routine analyses of soils for classification (e.g., particle size,

CEC, mineralogy); and fulfillment of experiments required by doctoral candidates.

Undergraduate teaching requirements included laboratory preparation, preparation of

handout materials, grading, and academic tutoring.

Publications:

“Single laboratory validation of a method for the determination of phenols and phenates in

disinfectant formulations by liquid chromatography with UV detection,” JAOACI

93(3):1039-1045, 2010.

“Determination of Phenols and Phenates in Disinfectant Formulations by Liquid

Chromatography with UV Detection: Collaborative Study,” JAOACI 95(2): 411-418, 2012.

“Building an Integrated Laboratory System to Advance the Safety of Food and Animal

Feed,” International Journal of Regulatory Science, 2(1): 1-6, 2014.

“Determination of nightshade alkaloids in a “stew” by HPLC-MS/MS,” submitted Journal

of Food Protection, 2015.

“A comparison of ELISA and HPLC-MS/MS in the determination of melamine in canned

and dry pet foods,” submitted JAOACI, 2015.

References:

Available upon request.

AOAC OMB Meeting Book

241