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SPIFAN Expert Review Panel Report
October 2, 2012
Final
Iod‐02
Determination of Total Iodine in Foods and Dietary
Supplements Using Inductively Coupled Plasma–Mass
Spectrometry. Submitted by Covance
No calculation formula
Use different forms of iodine
Erik Konings
Guenther Raffler
Recommend for First Action
Official Methods
SM
status
Method
Method Title
Comments
Reviewer(s)
Recommendation
Inos‐39
Analysis of Free and Total myo‐Inositol in Foods, Feeds,
and Infant Formula by HPAEC‐PAD Including a Novel
Total Extraction Using Microwave‐Assisted Acid
Hydrolysis and Enzymatic Treatment. Submitted by
Covance Lab
Modify sample procedure
Soy base product is excluded
Resolve the phytate issue
Brendon Gill
Karen Schimpf
Recommend for First Action
Official Methods
SM
status
Method
Method Title
Comments
Reviewer(s)
Recommendation
Panto‐01
Pantothenic Acid (Vitamin B5) in Fortified Foods:
Comparison of a Novel Ultra‐Performance Liquid
Chromatography‐Tandem Mass Spectrometry Method
and a Microbiological Assay (AOAC Official Method
SM
992.07). Submitted by Nestlé
Reference is to 1846
John Austad
Jeanne Rader
Recommend for First Action
Official Methods
SM
status
Method
Method Title
Comments
Reviewer(s)
Recommendation
Carn‐01
Single‐Laboratory Validation of a Liquid
Chromatographic/Tandem Mass Spectrometric
Method for the Determination of Free and Total
Carnitine in Infant Formula and Raw Ingredients.
Submitted by Abbott Nutrition
Total used instead of free
Need data on reference material
John Austad
Brendon Gill
Recommend for First Action
Official Methods
SM
status
Method
Method Title
Comments
Reviewer(s)
Recommendation
VitC‐02
Determination of Vitamin C by HPLC with UV
Detection. Submitted by Abbott Nutrition
SLV data on SPIFAN matrices
documentation on separation of
Isoascorbic
John Austad
Brendon Gill
Recommend for First Action
Official Methods
SM
status
VitC‐03
Single Laboratory Validation – Vitamin C by UPLC‐UV
method for discussion by Working Group SPIFAN.
Submitted by Nestlé
Establish criteria for the separation of
Isoascorbic and ascorbic
SLV data on SPIFAN matrices
Column lifecycle
System suitability
Resolution criteria needs to be set
Guifeng Jiang
Jeanne Rader
Recommend for First Action
Official Methods
SM
status
AOAC OMB Meeting Book
303