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FOR EXPERT REVIEW PANEL USE ONLY

NOT FOR DISTRIBUTION

3

NRC 0.78 – 3.2 %

CCC 1.1 – 8.9

Reproducibility (RSD

R

): ---

System suitability

:

Calibration solutions of glucose (2 μg/mL – 300 μg/mL) and fructose (20 μg/mL – 1100 μg/mL) at 8

different levels, were prepared in triplicate all containing the chitobiose internal standard (at 600

μg/mL).

Recommendation:

The good agreement of results between the two laboratories also indicates that the method is

robust to resist the minor changes in protocols between the two labs.

I recommend to move the method to First Action.