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CALIBRATION/QC STANDARDS
CS 1 0.001
CS 2 0.002
CS 3 0.005
CS 4 0.01
CS 5 0.05
CS 6 0.1
In powder In liquid
QC Std ug/g (ug/mL)
MQL 0.01 0.001
QC-Low 0.025 0.0025
QC-Med 0 1 0 01
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MFA‐AOAC, 2015
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. .
QC-High 0.5 0.05
STANDARD CURVE DATA (3 DAYS)
%Accuracy
WS1 WS2 WS3 WS4 WS5 WS6
Day-1
1 104 99.9 91.5 105.9 96.5 101.5
2 103.7 100.1 92.2 106.6 96.6 101.4
Day-2
1 103 98.4 93.3 106.2 97.2 101.5
2 104 100 1 92 2 106 6 96 3 101 2. . . . .
Day-3
1 99 101.7 91.7 108.6 97 101.3
2 101.5 101.3 91.6 108.9 96.5 101
Compound
Correlation coefficient: r=0.999479, r^2=0.998959
Calibration curve:0.949233 * x+ -0.0152233
Response type: InternalStd (Ref2 ),Area * ( ISConc. / ISArea )
Curve ,Weighting:1/x,Axis
Residual
0.0
5.0
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MFA‐AOAC, 2015
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Conc
-0 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100
Response
-0.0
20.0
40.0
60.0
80.0
Conc
-5.0