92 / 142
3/17/2015
14
MDL SPIKE CHROMATOGRAM (0.01 ug/g POWDER)
100
MRMof 2 channels,ES-
212 > 182
03121510 Smooth(Mn,2x2)
QC1
3.895e+004
MFA-2NPH
4.05
4 74
100
MRMof 2 channels,ES-
216 > 186
03121510 Smooth(Mn,2x2)
QC1
3.198e+005
MFA-2NPH_IS
4.04
min
%
0
3.16
2.83 3.35
.
4.22
6.59
4.81
6.27
6.21
5.48
4.91
6.66
6.90
Proprietaryand confidential — do not distribute
© 2015 Abbott Laboratories
March17,2015
MFA‐AOAC, 2015
|
27
min
0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 6.00 6.50 7.00
%
0
“DERIVATIZATION” METHOD PERFORMANCE DATA
(3 DAYS ACCURACY/PRECISION DATA)
Sample In powder (ug/g) In RTF liquid (ug/g)
QC-MDL
0.01
0.001
QC-Low
0.025
0.0025
QC-Med
0.1
0.01
QC-High
0.5
0.05
MDL Calculation
t-value, 99% CI, (N-1) = 8 degrees of freedom
2.896
SD
0.56
Proprietaryand confidential — do not distribute
© 2015 Abbott Laboratories
March17,2015
MFA‐AOAC, 2015
|
28
LOD
1.4 ppb