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Single Lab Validation Report for GOS in Infant Formula and Adult Nutritionals

24

* Date = date of preparative separation

** Instrument = instrument used for quantification

Spike-Recovery: Sample 11 Child Formula Powder

GOS Spike Level Measured GOS Recovery Average RSD

(g/100g)

(g/100g)

(%)

(%)

(%)

11-02-2015 ICS 3000

0.021

0.019

90

11-02-2015 ICS 3000

0.021

0.017

79

18-02-2015 ICS 5000

0.021

0.014

69

18-02-2015 ICS 5000

0.021

0.018

87

09-06-2015 ICS 3000

0.021

0.022

100

09-06-2015 ICS 3000

0.021

0.025

117

11-02-2015 ICS 3000

0.133

0.117

88

11-02-2015 ICS 3000

0.133

0.115

87

18-02-2015 ICS 5000

0.139

0.119

86

18-02-2015 ICS 5000

0.139

0.117

84

10-06-2015 ICS 3000

0.135

0.109

81

10-06-2015 ICS 3000

0.135

0.112

83

11-02-2015 ICS 3000

0.371

0.337

91

11-02-2015 ICS 3000

0.371

0.340

92

18-02-2015 ICS 5000

0.378

0.324

86

18-02-2015 ICS 5000

0.378

0.342

90

10-06-2015 ICS 3000

0.375

0.284

76

10-06-2015 ICS 3000

0.375

0.289

77

11-02-2015 ICS 3000

0.593

0.507

85

11-02-2015 ICS 3000

0.593

0.520

88

18-02-2015 ICS 5000

0.616

0.497

81

18-02-2015 ICS 5000

0.616

0.521

85

10-06-2015 ICS 3000

0.599

0.497

83

10-06-2015 ICS 3000

0.599

0.508

85

Vivinal

85

8.5

Clasado

84

2.8

Vivinal

90

18.5

Clasado

85

3.3

Date* Instrument** GOS

GOS-02 SLV

FOR ERP USE ONLY

DO NOT DISTRIBUTE