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70

V

aclavik

et al

.:

J

ournal of

AOAC I

nternational

V

ol

.

99, N

o

.

1, 2016

Figure 2. Chromatograms and mass spectra at 100 mg/kg (low test concentration) in matrix M1 (powder). (A) Sildenafil and (B) tadalafil.

Candidates for 2016 Method of the Year

171