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1132 

Mottier et al.

: J

ournal of

AOAC I

nternational

Vol. 98, No. 4, 2015

Figure 2015.03D. LC-MS/MS chromatograms of a powdered soya-based infant formula unspiked and spiked at the

1 µg/kg (IS 10 µg/kg) level.

Enclosure 3 – LC-MS/MS chromatograms of a powdered soya-based infant formula

unspiked and spiked at the 1 µg/kg (IS 10 µg/kg) level

77 → 33

77 → 57

79 → 34 (Internal Std)

79 → 59 (Internal Std)

77 → 33

77 → 57

79 → 34 (Internal Std)

79 → 59 (Internal Std)

Infant Formula

Soya-based

LIMS 890000008560

Unspiked

Infant Formula

Soya-based

LIMS 890000008560

Spiked at 1 µg/kg

Figure 2015.03E. LC-MS/MS chromatograms of a powdered milk infant formula unspiked and spiked at the 1 µg/kg (IS

10 µg/kg) level.

Enclosure 4 – LC-MS/MS chromatograms of a powdered milk infant formula unspiked

and spiked at the 1 µg/kg (IS 10 µg/kg) level

Milk Infant Formula

LIMS 890000008562

Unspiked

Milk Infant Formula

LIMS 890000008562

Spiked at 1 µg/kg

77 → 33

77 → 57

79 → 34 (Internal Std)

79 → 59 (Internal Std)

77 → 33

77 → 57

79 → 34 (Internal Std)

79 → 59 (Internal Std)

Candidates for 2016 Method of the Year

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