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1134 Mottier et al. : Journal of AOAC I nternational Vol. 98, No. 4, 2015
in the nonspiked sample in micrograms per kg. ρSpiked is the
concentration of sodium fluoroacetate spiked in the sample in
micrograms per kg (calculated value).
The recovery rate should be between 70–120% when spiked
at the 1 µg/kg level.
References
(1) Commission Decision 2002/657/EC of 12 August
2002 implementing Council Directive 96/23/EC
concerning the performance of analytical methods and
the interpretation of results, Off. J. Eur. Commun. (2002)
L221, 8–36.
F/?uri=CELEX:32002D0657&rid=1
(2) SANCO/12571/2013: Guidance document on analytical quality
control and validation procedures for pesticide residues analysis
in food and feed,
guidance_documents/docs/qualcontrol_en.pdf
(3) AOAC SMPR 2015.001 J. AOAC Int. (future issue)
Candidates for 2016 Method of the Year
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