OMB Meeting Book_9-11-14 - page 126-127

4
Repeatability standard deviation
s(r)
1.0797
0.1503
0.0261
0.0301
0.0103
0.0936
0.0244
0.0234
0.0000
5
Reproducibility standard deviation
s(R)
2.3749
0.5014
0.1725
0.0909
0.0576
0.3575
0.0850
0.0878
0.0000
6
Repeatability relative standard deviation
RSD(r)
11.34
6.94
3.92
8.36
4.72
5.53
7.71
6.89
0.00
7
Reproducibility relative standard deviation
RSD(R)
24.95
23.16
25.88
25.22
26.39
21.12
26.87
25.83
0.00
8
HORRAT value
2.19
2.30
2.15
1.91
1.86
2.02
2.00
1.94
0.00
a
One laboratory excluded - Failed Cochran Test
b
Overall mean in mg/100g RTF for all samples except SRM 1849a. SRM 1849a overall mean in mg/kg powder.
Study name:
AOAC 2011.18 Determination of Myo-Inositol - Total
Study date:
7/24/2014
Study Reported Values
Seq.
Item
Symbol
Sample ID:
SRM 1849a
E29JVLV
D04HTCVV
CONTROL 11752572116 117257651Z
BLANK
00412RF00 00403RF00
1
Total number of laboratories
p
9
9
8
a
7
b
7
c
9
8
8
d
8
b
2
Total number of replicates
Sum(n(L))
20
20
16
16
16
20
18
18
18
3
Overall mean of all data (grand mean)
e
XBARBAR 421.8668
6.2730
4.9366
7.5273
4.0368
4.7104
3.4602
5.4234
5.1066
4
Repeatability standard deviation
s(r)
11.9189
0.1467
0.0696
0.0588
0.0380
0.1521
0.0659
0.0280
0.0990
5
Reproducibility standard deviation
s(R)
11.9189
0.4459
0.3020
0.2008
0.1236
0.3569
0.1281
0.2852
0.2831
6
Repeatability relative standard deviation
RSD(r)
2.83
2.32
1.41
0.78
0.94
3.22
1.90
0.51
1.94
7
Reproducibility relative standard deviation
RSD(R)
2.83
7.05
6.12
2.66
3.07
7.55
3.70
5.23
5.56
8
HORRAT value
0.44
0.82
0.69
0.32
0.33
0.84
0.39
0.60
0.63
a
One
laboratory excluded - Failed Cochran and Double Grubbs Tests
b
One laboratory excluded - Failed Cochran Test
c
Two laboratory excluded - Failed Double Grubbs Test
d
One laboratory excluded - Failed Cochran and Single Grubbs Test
e
Overall mean in mg/100g RTF for all samples except SRM 1849a. SRM 1849a overall mean in mg/kg powder.
Value
1...,110,111,112,113,114,116-117,118-119,120-121,122-123,124-125 128-129,130-131,132,133,134,135,136,137,138,139,...
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