OMB Meeting Book_9-11-14 - page 128-129

7/24/2014 Copyright 2006,2012 by AOAC International, all rights reserved.
AOAC International Interlaboratory Study Workbook
Version:
2.1
All MLT Data Included
Blind (Unpaired) Replicates
Study name:
AOAC 2011.18 Determination of Myo-Inositol - Unbound
NO OUTLIERS REMOVED
Study date:
7/24/2014
Study Reported Values
Seq.
Item
Symbol
Sample ID:
SRM 1849a
E29JVLV D04HTCVV CONTROL 1172572116 117257651Z
BLANK
00412RF00 00403RF00
1
Total number of laboratories
p
10
10
10
9
10
10
9
10
10
2
Total number of replicates
Sum(n(L))
22
22
20
20
22
22
20
22
22
3
Overall mean of all data (grand mean)
a
XBARBAR 412.2442
4.2177
4.2629
7.1680
3.6532
3.1110
3.1705
5.1038
5.1024
4
Repeatability standard deviation
s(r)
11.3190
0.1273
0.1685
0.0953
0.0352
0.0899
0.0582
0.1847
0.2268
5
Reproducibility standard deviation
s(R)
11.3709
0.3051
0.2316
0.2071
0.4119
0.3889
0.0910
0.2462
0.3179
6
Repeatability relative standard deviation
RSD(r)
2.75
3.03
3.95
1.33
0.97
2.92
1.84
3.61
4.45
7
Reproducibility relative standard deviation
RSD(R)
2.77
7.26
5.43
2.89
11.35
12.61
2.87
4.81
6.24
8
HORRAT value
0.43
0.80
0.60
0.34
1.22
1.32
0.30
0.54
0.71
a
Overall mean in mg/100g RTF for all samples except SRM 1849a. SRM 1849a overall mean in mg/kg powder.
Study name:
AOAC 2011.18 Determination of Myo-Inositol - Phosphatidylinositol
NO OUTLIERS REMOVED
Study date:
7/24/2014
Study Reported Values
Seq.
Item
Symbol
Sample ID:
SRM 1849a
E29JVLV D04HTCVV CONTROL 1172572116 117257651Z
BLANK
00412RF00 00403RF00
1
Total number of laboratories
p
9
9
9
8
9
9
8
9
9
2
Total number of replicates
Sum(n(L))
20
20
18
18
20
20
18
20
20
3
Overall mean of all data (grand mean)
a
XBARBAR
9.5122
2.0962
0.6667
0.3476
0.2139
1.6418
0.3048
0.3282
0.0000
Value
Value
1...,111,112,113,114,116-117,118-119,120-121,122-123,124-125,126-127 130-131,132,133,134,135,136,137,138,139,140,...
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