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30

of

38

Table L: 3M

MDA

Salmonella

Presumptive vs. 3M

MDA

Salmonella

Confirmed – POD Results 375 g Raw Ground Beef

Matrix

Analyte Inoculum Level N

a

Presumptive

Confirmed

dPOD

CP

e

95% CI

f

X

b

POD

CP

c

95% CI

x

POD

CC

d

95% CI

10 Hours

Salmonella

enterica ser.

Anatum

ATCC

g

9270

Un-inoculated

5

0

0.00

0.00, 0.43

0

0.00

0.00, 0.43

0.00

-0.43, 0.43

Low

20

15

0.75

0.53, 0.89

15

0.75

0.53, 0.89

0.00

-0.26, 0.26

High

5

5

1.00

0.57, 1.00

5

1.00

0.57, 1.00

0.00

-0.43, 0.43

12 Hours

Salmonella

enterica ser.

Anatum

ATCC 9270

Un-inoculated

5

0

0.00

0.00, 0.43

0

0.00

0.00, 0.43

0.00

-0.43, 0.43

Low

20

15

0.75

0.53, 0.89

15

0.75

0.53, 0.89

0.00

-0.26, 0.26

High

5

5

1.00

0.57, 1.00

5

1.00

0.57, 1.00

0.00

-0.43, 0.43

18 Hours

Salmonella

enterica ser.

Anatum

ATCC 9270

Un-inoculated

5

0

0.00

0.00, 0.43

0

0.00

0.00, 0.43

0.00

-0.43, 0.43

Low

20

15

0.75

0.53, 0.89

15

0.75

0.53, 0.89

0.00

-0.26, 0.26

High

5

5

1.00

0.57, 1.00

5

1.00

0.57, 1.00

0.00

-0.43, 0.43

a

N = Number of test portions

b

x = Number of positive test portions

c

POD

CP

=

Candidate method presumptive positive outcomes divided by the total number of trials

d

POD

CC

= Candidate method confirmed positive outcomes divided by the total number of trials

e

dPOD

CP

= Difference between the candidate method presumptive result and candidate method confirmed result POD values

f

95% CI = If the confidence interval of a dPOD does not contain zero, then the difference is statistically significant at the 5% level

g

ATCC = American Type Culture Collection

2013.09 /PTM Matrix Extension Report

March 2014

Expert Review Panel Use Only

AOAC Research Institute

Expert Review Panel Use Only