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3/9/2017

4

Supporting Data including Method Optimization, Analytical

Ranges, Accuracy and Recovery, Precision, Reproducibility and System

Suitability

SUMMARY OF METHOD INCLUDING METHOD SCOPE/APPLICABILITY

Single-laboratory validation:

the methodology study of this high-throughput

technique experienced

9 stages

for 4 years from 2009-2013, with

511929 data

obtained, and

7 papers were published in J. AOAC Int.

Verification of EU standards against pesticide identifying applicability

in AOAC collaborative study

Study on the stability of mixed standard solutions of 460 pesticides

Study on the stability of 340 pesticides in tea

Study on the stability of 271 pesticides in tea Youden pair samples

Ruggedness Verification of Ruggedness of the method by designing 8

different analytical procedures for 210 pesticides

probe into the deviation ratios of predicted values of dynamic

degradation equation with actual values

16 laboratories attended simulated AOAC collaborative study

Using field trials to study pesticide degrading regularities in tea and

stabilities of tea incurred samples

2008.11.26-2009. 02. 26

28520 data

2009.03.31-2009.06.31

81420data

2009. 07.09-2009.10.09

129800 data

2011.10.27-2012.9.13

19920 data

2011.1.27-2011.3.8

19937 data

2010.09.12-12.24

10944 data

2010.05.13-2010.08.12

47216

data

2009.11.09-2010.02.07

189744 data

2012.10-2013.09:

24624 data

A Comparative Study on the Influences of Tea Hydration for the Method

Efficiencyof Pesticide Multiresidues