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5. Based on the supporting

information, what are the

cons/weaknesses of the

method?

6. Any general comments

about the method?

Do you recommend this

method be adopted as a First

Action and published in the

Official Methods of Analysis

of AOAC INTERNATIONAL?

Please specify rationale.

Internal standards need to be used prior extraction rather than post extraction.

method may be crosschecked with other equivalent make of instrument to confirm the

robustness of the method

Yes however thorough recovery studies shall be performed by using addition of

internal standards prior to the extraction .

SRM need to be verified and reported against actual values.

V. Final Recommendation