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Memo

Monique Steegmans

16001n-MSS-MSS-SLV FOS01 AOAC997.08 Beneo-Orafti, 1 Febr 2016, page 9/18

Raw material

spike concentration

g/100g reconstituted

product

Nutraflora

P95 HP

0,05

1 5

SRM 1849a

CLC10-b

x

x

infant powder partially

hydr Milk based

1172572116

x

x

infant powder partially

hydr Soy based

117257651Z

x

x

Adult powder low fat

00394RF00

x

x

Infant elemental powder

00403RF00

x

x

Infant formula milk based D04HTCVV

x

x

Infant formula powder

Soy based

E29JVLV

x

x

Infant formula RTF Milk

based

SPIFAN

Control milk

form EV4H2R

x

x

Adult nutr RTF high

Protein

00730RF00

x

x

Each spiked sample was analyzed in duplicate on 3 different days and handled by different

operators. Results can be found under point 3.2 and in annex 5.

3. Results

3.1 Precision

The standard performance requirement 2014.002 stated an analytical range of 0.03 to 5.0 g/100g

reconstituted final product and a repeatability (RDS

r

)

6%.

All products from the Test Materials Kit were screened for fructans and 4 products were positive.

Each sample was analyzed in double on 6 different days so 12 analyses in total per sample.

Product

SPIFAN

Code

ID

number

Fructan

g/100g*

RSD

r

%

RSD

iR

%

Adult nutr powder Milk Protein based

11750017V3

J4G-

00019

0,59

3,2

3,7

Adult nutr RTF high Fat

00729RF00

J4G-

00980

0,06

8,0

9,7

Child formula powder

00411RF00

J4G-

00013

0,35

4,5

4,8

Child formula powder

00412RF00

J4G-

00974

0,28

9,5

10,1

Average

6,3

7,1

*Fructan results are expressed in g/100 g reconstituted final product.

Fos-01 (February 2016)

FOR ERP USE ONLY

DO NOT DISTRIBUTE