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100

THE

COMPLETE

PRACTICAL

DISTILLER.

this

twice

more,

drawing

off

two-thirds

each

time

;

to

add

water

to

this

alcohol,

which

will

turn

'it

milky,

by

separat-

ing

the

essential

oil

remaining

in

it;

to

distil

the

spirit

from

this

water,

and

finally

rectify

it

by

one

or

more

dis-

tillations.

Others

set

apart the

first

running,

when

about

one-fourth

is

come

over,

and

continue

the

distillation

till

they

have

drawn

off

about

as

much

more,

or

till

the

liquor

runs

off

milky.

The

last

running

they

put

into

the

still

again,

and

mix

the

first

half

of

what

comes

over

with

the

preceding

first

product.

This

process

they

repeat

again,

when

all

the

first

products

mixed

together

are

distilled

afresh.

When

half

of

the

liquor

has

come

over,

this

is

to

be

set

apart

as

pure

alcohol.

Alcohol

in

this

state,

notwithstanding,

is

not

so

pure

as

when

it

has

been

dephlegmed,

or

still

fur-

ther

freed

from

water,

by

means

of

some

alkaline

salt.

Muriate

of

soda

has

been

recommended

for

this

purpose,

deprived

of

its

water

of

crystallization

by

heat,

and

added

hot

to

the

spirit

;

but

the

subcarbonate

of

potash

is

pre-

ferable.

About

a

third

of

the

weight

of

the

alcohol

should

be

added

to

it

in

a

glass

vessel,

well

shaken

and

then

suf-

fered

to

subside.

The

salt

will

be

moistened

by

the

water

absorbed

from

the

alcohol,

which

being

decanted,

more

of

the

salt

is

to

be

added;

and

this

is

to

be

continued

till

the

salt

falls

dry

to

the

bottom

of

the

vessel.

The

alco-

hol, in

this

state,

will

be

reddened

by

a

portion

of

pure

potash

which

it

will

hold

in

solution,

from

which

it

must

be

freed

by

distillation

in

a

water-bath.

Dry

muriate

of

lime

may

be

substituted

advantageously

for

the

alkali.

Lastly,

as

alcohol

is

much

lighter

than

water,

its

specific